Degradable plastic film capable of preserving freshness and visually monitoring freshness of seafood and preparation method of degradable plastic film
A technology for degrading plastics and freshness, which is applied in sustainable manufacturing/processing, sustainable packaging, climate sustainability, etc. It can solve the problems of visual freshness monitoring and visualization, and achieve pollution prevention and strong anti-oxidation effect of ability
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[0033] A preparation method of a degradable plastic film with freshness preservation and visual monitoring of seafood freshness, comprising the following steps:
[0034] (1) Extraction of cane peel anthocyanins from sugarcane peel: Dry the sugarcane peel in a constant temperature drying oven at 40-50°C to constant weight. After drying, pulverize the sugarcane peel into powder. The particle size of the powder is 40-60 mesh, and the powder After mixing with acidified ethanol in a mass ratio of 1:(20~25), stir at 40~50℃ for 1~3h, carry out vacuum filtration, and then the filtrate is concentrated by rotary evaporation in the dark at 40~50℃ to obtain concentrated The concentrated solution was vacuum freeze-dried for 24-48 hours to obtain cane peel anthocyanins, which were stored at 4°C in the dark. The volume ratio of acid solution to ethanol in the acidified ethanol is (1-1.5):4. The acid solution is one of acetic acid solution, oxalic acid solution and butyric acid solution, and...
Embodiment 1
[0042] The sugarcane peel is dried to constant weight in a constant temperature drying oven at 40°C. After drying, the sugarcane peel is pulverized into powder. The particle size of the powder is selected as 40 mesh, and the acidified ethanol prepared from 20ml of 1mol / L acetic acid solution and 80ml of ethanol is prepared. After mixing 40 g of powder with 2 g of powder, stirred at 40 °C for 3 hours, vacuum filtered, and then the filtrate was concentrated by rotary evaporation at 40 °C in the dark to obtain a concentrated solution, and the concentrated solution was vacuum freeze-dried for 48 hours to obtain cane peel anthocyanins, The cane peel anthocyanins were stored at 4°C in the dark. The sucrose was anaerobic fermented by lactobacillus at 38°C and pH 5.5, then ethyl acetate was added for extraction, the extract was distilled under reduced pressure at normal temperature, and 100 g of undistillate was added to the stirred tank reactor, Add 0.5g of titanium catalyst, raise t...
Embodiment 2
[0044] The sugarcane peel was dried to constant weight in a constant temperature drying oven at 45°C. After drying, the sugarcane peel was pulverized into powder. The particle size of the powder was 50 mesh, and 26ml of 1mol / L oxalic acid solution was mixed with 80ml of ethanol to prepare acidified ethanol. After mixing 46 g of powder with 2 g of powder, stirred at 45 °C for 2 h, vacuum filtered, and then the filtrate was concentrated by rotary evaporation at 45 °C in the dark to obtain a concentrated solution, and the concentrated solution was vacuum freeze-dried for 36 h to obtain cane peel anthocyanin, The cane peel anthocyanins were stored at 4°C in the dark. The sucrose was anaerobic fermented by lactobacillus at 40°C and pH 6.0, then ethyl acetate was added for extraction, the extract was distilled under reduced pressure at normal temperature, and 100 g of undistillate was added to the stirred tank reactor, Add 1.25g of titanium catalyst, raise the temperature to 215°C a...
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