Aluminum foil for ultraviolet reflecting material and preparation method of aluminum foil
A technology of ultraviolet light and aluminum foil, which is applied in the direction of reflection/signal paint, coating, special surface, etc., and can solve problems such as the decline of the ability to reflect ultraviolet light and the darkening of the color of aluminum foil
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Embodiment 1
[0039] The present embodiment is a preparation method of a stabilizer, comprising the following steps:
[0040] A1: Add 20.0g of paraformaldehyde and 1000mL of glacial acetic acid into a three-necked flask equipped with a stirrer, an air pipe and a reflux condenser, and feed hydrogen chloride while stirring at a temperature of 25°C and a stirring rate of 300r / min. gas for 30min, then add 100mL of 2,6-di-tert-butylphenol solution to form 2,6-di-tert-butylphenol solution formed by dissolving 2,6-di-tert-butylphenol in 20mL of glacial acetic acid according to 0.1mol, and then continue to pass Add hydrogen chloride gas for 40min, after the reaction is completed, the reaction product is allowed to stand for liquid separation, the organic phase is added to benzene, and then washed 2 times with saturated sodium chloride, saturated sodium bicarbonate solution and 8% sodium bicarbonate solution in mass fraction, Then stand for layering, the organic phase is dried with anhydrous magnesi...
Embodiment 2
[0045] The present embodiment is a preparation method of a stabilizer, comprising the following steps:
[0046] A1: Add 20.0g of paraformaldehyde and 1000mL of glacial acetic acid to a three-necked flask equipped with a stirrer, an air pipe and a reflux condenser, and feed hydrogen chloride while stirring at a temperature of 28°C and a stirring rate of 350r / min. Gas for 35min, then add 100mL of 2,6-di-tert-butylphenol solution to form 2,6-di-tert-butylphenol solution formed by dissolving 2,6-di-tert-butylphenol in 20mL of glacial acetic acid according to 0.1mol, and then continue to pass Into hydrogen chloride gas for 45min, after the reaction is completed, the reaction product is allowed to stand for liquid separation, the organic phase is added to benzene, and then washed 2 times with saturated sodium chloride, saturated sodium bicarbonate solution and a 9% sodium bicarbonate solution in mass fraction, Then stand for layering, the organic phase is dried with anhydrous magnes...
Embodiment 3
[0051] The present embodiment is a preparation method of a stabilizer, comprising the following steps:
[0052] A1: Add 20.0g of paraformaldehyde and 1000mL of glacial acetic acid into a three-necked flask equipped with a stirrer, an air pipe and a reflux condenser, and feed hydrogen chloride while stirring at a temperature of 30°C and a stirring rate of 400r / min. Gas for 40min, then add 100mL of 2,6-di-tert-butylphenol solution to form 2,6-di-tert-butylphenol solution formed by dissolving 2,6-di-tert-butylphenol in 20mL of glacial acetic acid according to 0.1mol, and then continue to pass Into hydrogen chloride gas for 50min, after the reaction is completed, the reaction product is allowed to stand for liquid separation, the organic phase is added to benzene, and then washed 3 times with saturated sodium chloride, saturated sodium bicarbonate solution and a 10% sodium bicarbonate solution in mass fraction, Then stand for layering, the organic phase is dried with anhydrous mag...
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