Peanut shell-based biochar material for adsorbing aflatoxin as well as preparation method and application of peanut shell-based biochar material
A kind of technology of aflatoxin and peanut shell, which is applied in the direction of chemical instruments and methods, fat production, and other chemical processes, can solve the problems that the safety of aflatoxin needs to be further studied, and achieve the effect of rich pores and large specific surface area
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Embodiment 1
[0049] A peanut shell-based biochar material for absorbing aflatoxin, the preparation method is as follows:
[0050] (1) Rinse the peanut shells with tap water 2-3 times to remove impurities and ash, then dry, pulverize, sieve, bag, and store in a desiccator in a 110°C oven for later use.
[0051] (2) Weigh 10g of crushed peanut shells in a crucible, add 2g of K 2 CO 3 (peanut shell and K 2 CO 3 The mass ratio of 5:1), add water, stir evenly, and dry in an oven at 110 °C.
[0052] (3) with the peanut shell after above-mentioned drying and K 2 CO 3 The mixture was placed in a high-temperature muffle furnace, carbonized at 340 °C for 1.5 h, and then heated to 700 °C for activation for 1.5 h.
[0053] (4) The sample after the reaction is taken out from the muffle furnace, washed with deionized water for cooling to pH 7-8, dried at 110° C., and cooled to obtain peanut shell-based biochar material for adsorbing aflatoxin .
Embodiment 2
[0055] A peanut shell-based biochar material for absorbing aflatoxin, the preparation method is as follows:
[0056] (1) Rinse the peanut shells with tap water 2-3 times to remove impurities and ash, then dry, pulverize, sieve, bag, and store in a desiccator in a 110°C oven for later use.
[0057] (2) Weigh 10g of crushed peanut shells in a crucible, add 4g of K 2 CO 3 (peanut shell and K 2 CO 3 The mass ratio of 5:2), add water, stir evenly, and dry in an oven at 110 °C.
[0058] (3) with the peanut shell after above-mentioned drying and K 2 CO 3 The mixture was placed in a high-temperature muffle furnace, carbonized at 340 °C for 1.5 h, and then heated to 700 °C for activation for 1.5 h.
[0059] (4) The sample after the reaction is taken out from the muffle furnace, washed with deionized water for cooling to pH 7-8, dried at 110° C., and cooled to obtain peanut shell-based biochar material for adsorbing aflatoxin .
Embodiment 3
[0061] A peanut shell-based biochar material for absorbing aflatoxin, the preparation method is as follows:
[0062] (1) Rinse the peanut shells with tap water 2-3 times to remove impurities and ash, then dry, pulverize, sieve, bag, and store in a desiccator in a 110°C oven for later use.
[0063] (2) Weigh 10g of crushed peanut shells in a crucible, add 6g of K 2 CO 3 (peanut shell and K 2 CO 3 The mass ratio of 5:3), add water, stir evenly, and dry in an oven at 110 °C.
[0064] (3) with the peanut shell after above-mentioned drying and K 2 CO 3 The mixture was placed in a high-temperature muffle furnace, carbonized at 340 °C for 1.5 h, and then heated to 700 °C for activation for 1.5 h.
[0065] (4) The sample after the reaction is taken out from the muffle furnace, washed with deionized water for cooling to pH 7-8, dried at 110° C., and cooled to obtain peanut shell-based biochar material for adsorbing aflatoxin .
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