Method for continuously producing high-purity o-chlorotoluene by adsorption separation method
A high-purity o-chlorotoluene technology, applied in the field of continuous production of high-purity o-chlorotoluene by adsorption separation, can solve the problems of inability to obtain high-purity o-chlorotoluene, avoid recovery steps, reduce processing costs, and simplify the process. line effect
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Embodiment 1
[0031] Take 50 g of o-chlorotoluene solutions of different production batches, add different types of molecular sieve adsorbents, stir at room temperature for a certain period of time, filter, analyze the mass fraction of o-chlorotoluene in the filtrate, and compare the adsorption effects of different adsorbents. The results are shown in Table 1. Show. It shows that the above molecular sieve adsorbents can selectively adsorb p-chlorotoluene in the o-chlorotoluene solution to obtain o-chlorotoluene with a mass fraction of ≥99.95%.
[0032] Table 1. Adsorption effects of different molecular sieve adsorbents
[0033]
Embodiment 2
[0035] like figure 1As shown, a system for continuous production of high-purity o-chlorotoluene by an adsorption separation method includes a first tubular adsorption tower 4 and a second tubular adsorption tower 5 connected in parallel, an o-chlorotoluene raw material storage tank 7, an adjacent Chlorotoluene product tank 8, toluene storage tank 6, condenser 9; the pipe-side inlets of the first row of tubular adsorption towers 4 are respectively connected with the o-chlorotoluene raw material storage tank 7 through the first ortho-chlorotoluene feed pipeline, and are connected through the first ortho-chlorotoluene feed pipeline respectively. A desorbent feed line is connected to the toluene storage tank 6, the first desorber feed line is connected to the blower 3 for feeding nitrogen into the tube path of the first tubular adsorption tower 4, the first The tube-side outlets of a row of tubular adsorption towers 4 are respectively connected to the o-chlorotoluene product tank ...
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