Preparation method of room temperature cured high temperature tolerant flexible epoxy adhesive
A high temperature resistant, flexible epoxy technology, applied in the direction of adhesive type, adhesive, epoxy resin, etc., can solve the problem, can only be used in the environment of 100 ~ 150 ℃, can not meet the strength, can not be cured, etc. problems, to achieve the effect of simple and convenient use, high impact strength, and high use temperature
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Embodiment 1
[0029] A. The composition of the toughening component and the temperature-resistant component in the adhesive component is calculated in parts by weight.
[0030] a. The composition of the toughening component:
[0031] Epoxy resin E51 100 parts
[0032] 20 parts of liquid-terminated carboxylated nitrile rubber
[0033] 30 parts liquid end hydroxy nitrile rubber
[0034] 4,4 diaminodiphenylmethane tetrafunctional epoxy resin 10 parts
[0035] b. Composition of temperature-resistant components:
[0036] Epoxy resin E20 80 parts
[0037] Temperature-resistant modifier 50 parts
[0038] Silicone resin 50 parts
[0039] Phenolic resin F648 48 parts
[0040] Among them, the silicone resin is synthesized and prepared by itself from 40 parts of diphenyldichlorosilane, 10 parts of dimethyldichlorosilane and 3 parts of boric acid.
[0041] B. The composition of the curing component in terms of the same weight unit parts is as follows:
[0042] a. Main curing agent
[0043] Po...
Embodiment 2
[0062] A. The composition of the toughening component, the temperature-resistant component and the plasticizer in the adhesive component are all calculated in the same weight unit.
[0063] a. The composition of the toughening component:
[0064] Epoxy Resin-E50 100 parts
[0065] Liquid end carboxyl nitrile rubber 40 parts
[0066] 4,4 diaminodiphenylmethane tetrafunctional epoxy resin 5 parts
[0067] Resorcinol functional epoxy resin 6 parts
[0068] b. Composition of temperature-resistant components:
[0069] Epoxy resin E20 90 parts
[0070] Silicone resin 60 parts
[0071] Phenolic resin F648 40 parts
[0072] c. Plasticizer
[0073] 2 parts dibutyl phthalate
[0074] B. The composition of the curing component in terms of the same weight unit parts is as follows:
[0075] a. Main curing agent
[0076] Polyetheramine 100 parts
[0077] b. Curing accelerator
[0078] Hexamethylenediamine 6 parts
[0079] Dicyandiamide 6 parts
[0080] 4 parts of 2-ethyl-methy...
Embodiment 3
[0087] A. The composition of the toughening component, the temperature-resistant component and the plasticizer in the adhesive component are all calculated in the same weight unit.
[0088] a. The composition of the toughening component:
[0089] Epoxy Resin-E51 100 parts
[0090] Liquid end carboxyl nitrile rubber 25 parts
[0091] 20 parts liquid end hydroxy nitrile rubber
[0092] 7 parts of 4,4 diaminodiphenylmethane tetrafunctional epoxy resin
[0093] Resorcinol difunctional epoxy resin 4 parts
[0094] b. Composition of temperature-resistant components:
[0095] Epoxy resin (E20) 100 parts
[0096] Silicone resin (self-synthesized) 60 parts
[0097] Phenolic resin (F648) 45 parts
[0098] Among them, the silicone resin is prepared by self-synthesis from 50 parts of diphenyldichlorosilane, 10 parts of dimethyldichlorosilane and 5 parts of boric acid.
[0099] c. Plasticizer
[0100] 5 parts dibutyl phthalate
[0101] B. The composition of the curing component i...
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