Waste water purifying agent, and its preparing method and use
A purifying agent and wastewater technology, which is applied in chemical instruments and methods, water/sewage treatment, adsorbed water/sewage treatment, etc. It can improve the ability of removing oil pollution and various harmful impurities, improve the separation rate of free water, and improve the lipophilicity.
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[0057] Example 1
[0058] Cationized Attapulgite A1 Preparation:
[0059]a. Sodium treatment: pulverize the attapulgite into 150 meshes to be fine, and mix it with a sodium chloride (NaCl) solution with a concentration of 150g / l. The weight ratio of NaCl to attapulgite is preferably 3:1. After fully stirring for 8h, solid-liquid separation is carried out, and the precipitate is washed, dried at 110°C, and crushed through a 200-mesh sieve.
[0060] b. Electrical modification treatment: the sodium-treated attapulgite and aluminum chloride (AlCl3) solution with a concentration of 0.5 mol / l are thoroughly mixed. The weight ratio of AlCl3 to attapulgite is preferably 1:1. After fully stirring for 24h, solid-liquid separation is carried out, and the precipitate is washed, dried at 110°C, and crushed through a 200-mesh sieve.
[0061] c. Pore-forming treatment: The paper scraps that have passed through a 60-mesh sieve are mixed with polyvinyl alcohol in a weight ratio of 2:1 as a porogen...
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[0063] Example 2
[0064] Preparation of activated alumina B1:
[0065] a. Wash and dry glass and ceramics separately.
[0066] b. Crush the above glass and ceramics through a 200 mesh sieve.
[0067] c. Mix the ceramic powder and glass powder in a ratio of 3:1 to obtain the activated alumina B2 .
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[0068] Example 3
[0069] Activated silicate B2 Preparation:
[0070] a. Take commercially available water glass (Na 2 SiO 3 Or K 2 SiO 3 ), which is Na 2 O·nSiO 2 Or K 2 O·nSiO 2 , Where n is greater than or equal to 3. Press Al +3 : SiO 2 The water glass and the aluminum hydroxide solution are thoroughly mixed uniformly at a molar ratio of 1:1.
[0071] b. Add 15% sulfuric acid dropwise to the above mixture to adjust the pH to 3.6, and continue to stir for 8 hours. Then solid-liquid separation is performed. 15% sulfuric acid was used as the acid.
[0072] c. Dry the solid phase obtained in step b at 300°C for 2 hours, then cool and pulverize to obtain the activated silicate B2 .
[0073] 2. Wastewater purification agent preparation and water treatment experiment
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