Method for measuring size distribution of grains in Nano level through method of capillary electrophoresis

A capillary electrophoresis, nano-scale technology, applied in the direction of particle and sedimentation analysis, particle size analysis, measuring devices, etc., can solve the problems of difficult quantitative and statistical analysis, high laser source price, high instrument price, etc., to achieve simple structure and easy operation line, low cost effect
CN1727873AInactive Publication Date: 2006-02-01CHINA PETROLEUM & CHEM CORP +1

Patent Information

Authority / Receiving Office
CN · China
Current Assignee / Owner
CHINA PETROLEUM & CHEM CORP
Publication Date
2006-02-01
Estimated Expiration
Not applicable · inactive patent

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Abstract

A method for determining particle size distribution of nanoparticle by utilizing capillary tube electrophoresis includes preparing nanoparticle sample to be suspension , obtaining capillary tube electrophoretic spectrogram of suspension through separation and detection , substituting regulation moving time of particle with different particle size in spectrogram in correlation equation of particle ¿C regulation moving time for obtaining particle size value , calibrating absorbance obtained from spectrogram with calibration equation of particle content scattering for obtaining content percentage of particle with different particle size .
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Description

technical field

[0001] The invention is a method for measuring the size distribution of nanoscale particles, specifically, a method for separating particles with different particle sizes by capillary electrophoresis and then measuring the particle size distribution. Background technique

[0002] Due to its small particle size, large specific surface area and quantum size effect, nano-powder materials have special properties that conventional coarse-grained materials do not have, and exhibit outstanding performance in light absorption, light filtering, catalysis and other functional properties. Eye-catching application prospects. The particle size and distribution have a great relationship with the overall performance of the material. Taking nanocatalyst as an example, the particle size and particle size distribution of nanocatalyst directly affect its catalytic performance. If the particle size distribution is very wide, or even only a small part of the particle size is at ...

Claims

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