High saturated magnetic flux density and low loss manganese-zinc ferrite material and its preparing method
A technology of manganese-zinc ferrite and magnetic flux density, applied in the direction of magnetism of inorganic materials, can solve the problems of easy agglomeration and high cost of raw materials, and achieve the effects of simple addition, simple preparation method and low cost
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Embodiment 1
[0058] 1) Raw material mixing:
[0059] Select 54mol% Fe 2 o 3 , 33mol% MnO and 13mol% ZnO as raw materials, put them into a ball mill, add deionized water of equal weight, and ball mill for 2 hours. 2 The content is controlled at about 25ppm.
[0060] 2) Pre-burning:
[0061] Dry the mixed and ground material, put it into the furnace for pre-burning, the pre-burning temperature is 950°C, and the pre-burning time is 3 hours.
[0062] 3) Addition of impurities:
[0063] Add auxiliary ingredients to the pre-fired powder, these auxiliary ingredients include:
[0064] make up
[0065] 4) Secondary ball milling:
[0066] Put the calcined material added with auxiliary components into a ball mill, add an equal weight of deionized water, and ball mill for 3 hours, so that the average particle size of the calcined material is 1.2 μm.
[0067] 5) Molding:
[0068] Dry the slurry, add 10wt% polyvinyl alcohol (PVA), and press it into a ring shape with an outer diameter o...
Embodiment 2
[0078] 1) Raw material mixing:
[0079]Select 52mol% Fe 2 o 3 , 40mol% MnO and 8mol% ZnO as raw materials, put them into a ball mill, add deionized water of equal weight, and ball mill for 5 hours. 2 The content is controlled at about 30ppm.
[0080] 2) Pre-burning:
[0081] Dry the mixed and ground material, put it into the furnace for pre-burning, the pre-burning temperature is 800°C, and the pre-burning time is 3 hours.
[0082] 3) Addition of impurities:
[0083] Add auxiliary ingredients to the pre-fired powder, these auxiliary ingredients include:
[0084] make up
[0085] 4) Secondary ball milling:
[0086] Put the calcined material with added auxiliary components into a ball mill, add an equal weight of deionized water, and ball mill for 6 hours, so that the average particle size of the calcined material is 1.0 μm.
[0087] 5) Molding:
[0088] Dry the slurry, add 10wt% polyvinyl alcohol (PVA), and press it into a ring shape with an outer diameter of ...
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