Method of preparing exo-dicyclopentadiene from endo-dicyclopentadiene or cyclopentadiene
A technology for dicyclopentadiene and cyclopentadiene, which is applied in the field of hanging type dicyclopentadiene preparation, can solve the problems of low yield and output, complex method and process, and achieves mild reaction conditions in liquid phase and high yield. Effect
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Embodiment 1
[0010] Reaction time
Embodiment 2
[0012] Add 200g of bridged dicyclopentadiene to 200g of benzene, and add 2,5-di-tert-butylhydroquinone with a mass content of 300ppm to the solution, at a temperature of 100°C and a pressure of 2.0MPa After reacting for 3 minutes, the conversion rate of bridge dicyclopentadiene was 15.2%, the selectivity of hanging dicyclopentadiene was 76.4%, and the yield was 11.6%. Alkenes 23.2g.
Embodiment 3
[0014] 100g cyclopentadiene is added in 1000g toluene, and temperature is 190 ℃, the reaction is 7 minutes under the condition of pressure 6.0MPa, and the conversion rate of cyclopentadiene is 95.1%, and the selectivity of hanging type dicyclopentadiene is 91.6%, the yield is 87.2%.
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