Antiseptic active cationic dye and its preparing method

A reactive dye and cationic technology, which is applied in the field of antibacterial cationic reactive dye and its preparation, can solve the problems of lack of affinity for cotton fiber, loss of antibacterial properties of dyes, easy hydrolysis and other problems, and achieve excellent antibacterial durability and excellent dyeing affinity.

Inactive Publication Date: 2007-06-27
DONGHUA UNIV
View PDF0 Cites 25 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the dye lacks affinity for cotton fibers, and because the quaternary ammonium salt in the molecule is combined

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Antiseptic active cationic dye and its preparing method
  • Antiseptic active cationic dye and its preparing method
  • Antiseptic active cationic dye and its preparing method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] a. Dissolve 17g of 1-aminoanthraquinone and 20g of trifluoro-s-triazine in 200ml of nitrobenzene organic solvent, heat the mixture to 90°C, and raise the temperature to 120°C after 1 hour, at this temperature Continue to stir for about 1 hour, cool to 25-30°C, filter to obtain the dye intermediate 1-(4,6-dichloro-2-amino-s-triazine)aminoanthraquinone, wash with methanol, and dry in a vacuum dryer;

[0019] b. the dye intermediate 1-(4,6-dichloro-2-amino-s-triazine) aminoanthraquinone 10g prepared in step a is dissolved in 150ml DMF (N,N-dimethylformamide) organic solvent, heated to 55°C, slowly drop 5.5 g of 1-amino-3-dimethylaminobutane in 30 minutes, and then react for 2 hours. After the reaction is complete, evaporate the solvent DMF in a vacuum evaporator to obtain the dye intermediate 1- (4-chloro-6-(1-amino-3-dimethylaminobutane) 2-amino-s-triazine) aminoanthraquinone, dried in a vacuum dryer;

[0020] c. Dissolve 9 g of the dye intermediate prepared in step b in...

Embodiment 2-21

[0024] Example 2-21, the synthesis method of the antibacterial cationic reactive dye is basically the same as that of Example 1, and see Table 1 for other conditions.

[0025] Table 1 Examples 2-21

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The present invention relates to one kind of antiseptic active cationic dye and its preparation process. The dye has matrix in anthraquinone structure, active group of sym-triazine monochloride or sym-triazine monofluoride, water soluble group of long carbon chain quaternary ammonium salt structure and the chemical structure as shown. The dye may be used in dyeing and antiseptic finishing of various kinds of fiber and has high antiseptic effect, high color fastness and lasting antiseptic performance. It is prepared through the following steps: dissolving anthraquinone A and sym-triazine trichloride or sym-triazine trifluoride in nitrobenzene solvent, heating, cooling and filtering to obtain intermediate B; dissolving the intermediate B in DMF solvent, adding tertiary amine, heating to react, evaporating DMF and vacuum drying to obtain intermediate D; dissolving the intermediate D in DMF solvent, adding alkyl halide, heating to react, washing with ethyl ether, re-crystallizing and drying.

Description

technical field [0001] The invention belongs to the fields of dye synthesis, textile dyeing and finishing, and in particular relates to an antibacterial cationic reactive dye and a preparation method thereof. Background technique [0002] Textile dyeing and finishing are two important wet processing processes, while traditional textile dyeing and finishing are carried out separately, which has the disadvantages of high cost, high energy consumption and large amount of sewage discharge. The dyeing and finishing technology that combines dyeing and functional finishing in one bath is of great significance for reducing production costs, saving energy, reducing waste water discharge, and protecting the ecological environment. Therefore, many experts at home and abroad have carried out a lot of research in this field, and have achieved certain results in the research of dyeing, antistatic, flame retardant, anti-ultraviolet, shrink-proof and anti-wrinkle finishing in one bath. How...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): C09B62/06D06P1/382D06P3/52D06P3/60D06P3/04D06P3/70
Inventor 赵涛王革辉
Owner DONGHUA UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap