High flow rate sampler for measuring emissions at process components
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example 1
y Validation Experiments
A series of experiments have been conducted to validate the results of the high flow rate sampler and to optimize the design. A simulated leak was used from which a known flow rate of methane was released.
The laboratory tests were conducted by releasing methane from a compressed gas cylinder through a two stage regulator and needle valve. The methane flow rate was measured using a one liter soap bubble meter (Alltech, Inc.) Methane flow rates were measured before and after each sampling period and had a nominal range of 0.5 l / min to 11 l / min. (All volumetric flow rates have been converted to conditions at 70.degree. F., 1 atm.) Two different diameters of tubing were used for the release configuration, one with 1 / 4" O.D. (approximately 3 / 16" I.D.) and one with 1 / 8" O.D. (approximately 3 / 32" I.D.). These different release diameters were used to investigate the effects of the leak exit velocity on the ability of the high flow sampler to completely capture the le...
example 2
onstration of the High Flow Sampler
As indicated previously, the high flow sampler allows an accurate emission rate to be made in less than one tenth the time required to perform an enclosure measurement. Consequently, the high flow sampler make it possible to accurately quantify leak emission rates from leaking components instead of estimating the emission rates from screening correlations. The implications are two fold. First, emissions can now be quantified far more accurately than was ever possible before. Previously it has been uneconomical to perform enclosure measurements at all leaking components or even at all the components which resulted in "pegged source" (off scale) screening values. Additionally, with the leak rate database that can be generated for a specific facility, the largest leaks can be targeted for priority repair. Generally, the majority of emissions result from a relative small fraction of the leaking components. Repair of the large leaks allows large (and qu...
example 3
n of present invention to existing techniques
To quantify the variation in the screening concentration as a function of wind speed, we made measurements under laboratory controlled conditions. Methane was released from a 1 / 16".times.0.004" flow restrictor secured to a 11 / 4" diameter pipe to simulate a methane leak at a component. The release rate was measured using a soap bubble meter. The release rate of methane was varied between 1.97 ml / min and 8.89 ml / min. Screening measurements were made at 1 mm and 1 cm sampling distances in still air (air movement <0.1 m / s) and at wind speeds generated by a 20" fan ranging from 1.0 to 1.6 m / s as measured by a vane anemometer. The results are shown in FIG. 4. At a sampling distance of 1 mm, the screening values are close to the theoretical 100% capture curve in both still air and when the fan was on. At a sampling distance of 1 cm, the screening values are still relatively close to the theoretical curve. However, when the fan was on, the screen...
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