Composition containing liquid fat phase and particle paste through gelatinization of semi-crystalline polymer
A technology of semi-crystalline polymers and compositions, applied in the direction of medical preparations containing active ingredients, body powders, skin care preparations, etc., which can solve problems such as strengthening the coated surface, causing problems, and being unsightly
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Embodiment 1
[0159] Example 1: Acidic polymer with a melting point of 40°C
[0160] 120 g of Parleam were added to a 1 liter reactor equipped with a central anchor stirrer, reflux condenser and thermometer and heated from room temperature to 80°C over 45 minutes. The following mixture C was added over 2 hours at 80 °C 1 : 40 g cyclohexane + 4 g Triganox 141 [2,5-bis(2-ethylhexanoylperoxy)-2,5-dimethylhexane]. After 30 minutes, in mixture C 1 Add mixture C over 1 hour and 30 minutes 2 , C 2 The composition is as follows: 190g stearyl acrylate + 10g acrylic acid + 400g cyclohexane. After the addition of both, the reaction mixture was allowed to continue at 80° C. for 3 hours, and then all cyclohexane in the reaction mixture was distilled off at atmospheric pressure. A polymer containing 60% by weight of active ingredient in Parleam is then obtained. Its weight average molecular weight M w It is 35000, characterized by polystyrene equivalent, and its melting temperature M.t. measured b...
Embodiment 2
[0161] Example 2: Basic polymer with a melting point of 38°C
Embodiment 3
[0163] Example 3: Acidic polymer with a melting point of 60°C
[0164] The same procedure as Example 1 was applied, but wherein behenyl acrylate was used instead of stearyl acrylate. The resulting polymer is 60% by weight active ingredient present in Parleam with a weight average molecular weight M w is 42000, and the melting point M.t. is 60°C.
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