Fortifying fiber auxiliary agent and manufacturing method thereof
A technology for reinforcing fibers and manufacturing methods, applied in the field of reinforcing fiber additives for composite materials and its manufacturing, to achieve the effects of easy popularization and application, easy use, and stable performance
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Embodiment 1
[0072] Add 50kg of starter dodecanoic acid and 2.0kg of catalyst (KOH) into the autoclave, vacuumize it, replace it with nitrogen 4 times, raise the temperature to 120°C, and inject 880kg of mixed EO (EO mole The number is 20), 580kgPO (PO mole number is 10), keep the reaction pressure at 0.3-0.4Mpa, continue to react until the pressure does not change, vent, cool down to 80°C, add 4.0kg of phosphoric acid and stir for 30min, add adsorbent to synthesize silicic acid Magnesium 1.0kg, continue stirring for 60 minutes, filter to obtain product A 1 .
[0073] Add 100kg ethylene glycol in reactor, add 2.5kg metal potassium (catalyst) again, start agitator simultaneously. After metal potassium in the reaction liquid is completely dissolved, add 600kg of octanol glycidyl ether into the reaction system, then heat the reaction liquid to above 60°C, and react for 10-20 hours. After the reaction is completed, the reaction mixture is distilled under reduced pressure to remove unreacted et...
Embodiment 2
[0076] Add 50kg of initiator dodecyl alcohol and 2.0kg of catalyst (KOH) into the autoclave, vacuumize it, replace it with nitrogen 4 times, raise the temperature to 120°C, and pass 880kg of mixed EO (EO mole The number is 20), 580kgPO (PO mole number is 10), keep the reaction pressure at 0.3-0.4Mpa, continue to react until the pressure does not change, vent, cool down to 80°C, add 4.0kg of phosphoric acid and stir for 30min, add adsorbent to synthesize silicic acid Magnesium 1.0kg, continue stirring for 60 minutes, filter to obtain product A 2 .
[0077] Add 100kg ethylene glycol in reactor, add 2.5kg metal potassium (catalyst) again, start agitator simultaneously. After metal potassium in the reaction solution completely disappears, add 600kg of glycidyl lauryl ether into the reaction system, then heat the reaction solution to above 60°C, and react for 10-20 hours. After the reaction is completed, the reaction mixture is distilled under reduced pressure to remove unreacted...
Embodiment 3
[0080] Add 100kg of starter palmitic acid and 2.0kg of catalyst (KOH) into the autoclave, vacuumize it, replace it with nitrogen 4 times, raise the temperature to 120°C, and feed the mixed 1320kg of EO under negative pressure (the moles of EO The number is 30), 580kgPO (the number of moles of PO is 10), keep the reaction pressure at 0.3-0.4Mpa, continue the reaction until the pressure does not change, vent, cool down to 80°C, add 4.0kg of phosphoric acid and stir for 30min, add an adsorbent to synthesize silicon Magnesium acid 1.0kg, continue to stir for 60 minutes, filter, can obtain product A 3 .
[0081] Add 100kg ethylene glycol in reactor, add 2.5kg metal potassium (catalyst) again, start agitator simultaneously. After metal potassium in the reaction solution completely disappears, add 600kg of octanol glycidyl ether into the reaction system, then heat the reaction solution to above 60°C, and react for 10-20 hours. After the reaction is completed, the reaction mixture i...
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