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865results about How to "Uniform dispersion" patented technology

SiOx based composite negative electrode material, preparation method and battery

The invention relates to a high-capacity SiOx based composite negative electrode material, a preparation method and a battery, wherein the negative electrode material comprises a silicon oxide material, a carbon material and an amorphous carbon coating layer; the silicon oxide material is silicon oxide or silicon oxide material modified in a carbon coating manner; surfaces of carbon material particles are coated with the silicon oxide material. A preparation method of the high-capacity SiOx based composite negative electrode material comprises the steps of performing physical processing or carbon coating modification on a silicon oxide raw material, thus obtaining a micron-sized silicon oxide material; and then mechanically fusing, coating with a solid phase and sintering at a high temperature to obtain the high-capacity negative electrode material. Through the high-capacity SiOx based composite negative electrode material, the effect of uniform dispersing and coating of the micron-sized silicon oxide particles on the surfaces of the carbon material particles can be achieved by virtue of the combination of mechanical fusion and solid-phase coating processes. The silicon oxide particles are well dispersed on the surface of the carbon material particle; the strength of bonding between the silicon oxide particles and the carbon material particles is high; the recycling performance of the material can be greatly improved; and meanwhile, the high-capacity SiOx based composite negative electrode material is high in first efficiency (breaking through the theoretical efficiency of SiOx), low in expansion rate, long in service life, environmental-friendly, pollution-free and low in cost.
Owner:BTR NEW MATERIAL GRP CO LTD

Water-soluble polymer/graphene composite fiber as well as preparation method and application thereof

The invention relates to water-soluble polymer/graphene composite fiber as well as a preparation method and application thereof. The cross section of the fiber is special-shaped, the surface of the fiber is of an orientated micro-fiber-shaped structure, the strength of the fiber is greater than 100 MPa, the elongation at break is greater than 2%, and the conductivity of the fiber is greater than 0.1 S/cm. The preparation method comprises the following steps: preparing a composite spinning liquid, extruding into a coagulating bath for curing, drafting, leading out of the coagulating bath, drying, and coiling, thereby obtaining the water-soluble polymer/graphene composite fiber; and finally reducing by using a chemical or physical method, thereby obtaining the water-soluble polymer/graphene composite fiber. The cross section of the composite fiber provided by the invention is of a special-shaped structure, the surface of the fiber is of a rich groove micro structure, the strength and the toughness of the fiber are greatly improved when being compared with those of pure graphene fiber, and good conductivity is still maintained, so that the water-soluble polymer/graphene composite fiber has a wide application prospect in the fields such as anti-electrostatic and conductive fabrics, electromagnetic wave absorption and shielding fabrics, energy storage devices, sensors and water treatment.
Owner:DONGHUA UNIV

Preparation method of high dispersion metal-organic framework (MOF)/organic hybrid priority alcohol through composite membrane

The invention relates to a preparation method of a high dispersion metal-organic framework (MOF) / organic hybrid priority alcohol through composite membrane, belonging to the technical field of membrane separation. The method comprises the steps of cleaning MOF crystal particles, and dispersing the cleaned crystal particles into a polar solvent without drying to form stable MOF emulsion; dissolving 0.5-5wt% of high-molecular polymer into a solvent, feeding the MOF emulsion, and then feeding a cross-linking agent and a catalyst to prepare membrane liquid A; dissolving 8-20wt% of high-molecular polymer into the solvent, and feeding the cross-linking agent and the catalyst to prepare membrane liquid B; dipping a base membrane into the membrane liquid A, taking out the base membrane and drying; dipping the surface of the base membrane for a plurality of times to obtain a nascent state MOF / high-molecular polymer hybrid separation layer; after that, dipping the base membrane into the membrane liquid B, taking out the base membrane and drying; putting into a vacuum oven to enable the high-molecular polymer to be completely cross-linked on the surface of the base membrane. The prepared hybrid composite membrane has excellent alcohol through performance and potential application value.
Owner:BEIJING UNIV OF TECH

Flame-resistant and heat-resistant copper clad laminate preparation method

The present invention relates to a flame-resistant and heat-resistant copper clad laminate preparation method, which comprises: adopting nanometer silica foam, dodecyl benzenesulfonic acid, bismuth nitrate pentahydrate, methyl trichlorosilane and polyoxyethylene sorbitan monooleate as a raw materials to obtain a filler; adopting DOPO, a bisphenol A cyanate ester monomer, a phenol compound, a m-nitrobenzene sulfonic acid pyridine salt, 2,3-epoxy cyclopentyl cyclopentyl ether and dimethyl phosphonate as raw materials to obtain a resin prepolymer; adding the filler to o-phthalic acid diglycidyl este to obtain an active filler; mixing the resin prepolymer and an indole compound, and then adding the active filler and isomeric undecanol polyoxyethylene ether phosphate potassium salt to obtain a composite system; and carrying out hot pressing molding on the composite system, a reinforced material and metal foil to obtain the flame-resistant and heat-resistant copper clad laminate, wherein the flame-resistant and heat-resistant copper clad laminate has characteristics of excellent flame retardant property and excellent heat resistance, and meets the development applications of the flame-resistant and heat-resistant copper clad laminate.
Owner:SUZHOU YIKETAI ELECTRONICS MATERIAL

Sodion-embedded manganese dioxide nanometer sheet electrode as well as preparation method and application of electrode

The invention relates to a sodion-embedded manganese dioxide nanometer sheet electrode as well as a preparation method and an application of the electrode. The electrode can be used as the active material of a supercapacitor and comprises sodion-embedded manganese dioxide nanometer sheets evenly distributed on the surface of a foamed nickel substrate. The preparation method comprises the following steps of: (1) mixing sodium sulfate and manganese acetate to prepare an electrochemical deposition precursor solution; (2) setting up an electrochemical deposition platform through a three-electrode method and taking the foamed nickel substrate after pretreatment as a working electrode, a platinum electrode as a counter electrode and a saturated calomel electrode as a reference electrode; (3) soaking the electrodes in the electrochemical deposition precursor solution at same depth; (4) opening an electrochemical workstation, setting the working electrode to the anode, setting the working mode to a timing potential mode, and starting up the electrochemical workstation; (5) taking out and washing the working electrode after the electrochemical workstation stops working; and (6) drying to obtain the sodion-embedded manganese dioxide nanometer sheet electrode. The sodion-embedded manganese dioxide nanometer film electrode as well as the preparation method and the application of the electrode disclosed by the invention have the characteristics of simple technique, mild reaction condition and excellent electrochemical performance of materials.
Owner:WUHAN UNIV OF TECH

Hetero atom-doped hollow spherical grapheme composite material, and preparation method and applications thereof

The invention belongs to the technical field of carbon material and electrochemistry, and discloses a hetero atom-doped hollow spherical grapheme composite material, and a preparation method and applications thereof. The preparation method comprises following steps: styrene, polyvinyl pyrrolidone, and 2,2'-azobis(2-methylpropionamidine) dihydrochloride are mixed with water, and positively charged polystyrene spheres are prepared under certain conditions; a graphene oxide aqueous dispersion and a positively charged polystyrene sphere aqueous dispersion are stirred for reaction so as to prepare a graphene oxide@polystyrene sphere compound; a hetero atom-doped sourced compound and a solvent are added into the graphene oxide@polystyrene sphere compound, and an obtained mixture is subjected to mixing, coating, and freeze drying so as to obtain solid thin films; a substrate loaded with the solid thin films is delivered into a plasma high-temperature tubular reactor for reaction so as to obtain the hetero atom-doped hollow spherical grapheme composite material. The hetero atom-doped hollow spherical grapheme composite material possesses relatively high specific surface area and relatively excellent electrical properties, and can be applied to the field of supercapacitor.
Owner:SOUTH CHINA UNIV OF TECH

Electroconductive slurry and preparation method thereof, and printed circuit material

The invention discloses electroconductive slurry and a preparation method thereof, and a printed circuit material. The electroconductive slurry comprises a polymer resin matrix and metal powder which is dispersed in the polymer resin matrix and serves as an electroconductive filler, wherein the microstructure of the metal powder is a three-dimensional dendritic metal crystal structure; the diameter of the metal crystal structure is 0.5-50 microns; a second-stage dendritic structure is 5 nanometers- 5 microns long. According to the electroconductive slurry and the preparation method thereof which are disclosed by the invention, the metal powder with the three-dimensional dendritic metal crystal structure serving as the microstructure is used as the electroconductive filler, so that the percolation threshold value of the electroconductive slurry can be greatly reduced, and the higher electroconductivity can be realized with less metal filler; furthermore, the metal powder with the three-dimensional dendritic metal crystal structure serving as the microstructure is used as the electroconductive filler, so that the electroconductive slurry can keep a high isotropous electroconduction effect and uniform dispersion; due to a nano-end structure, the resistivity of the electroconductive slurry can be greatly reduced, and the electroconductivity can be improved.
Owner:SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV

Lithium ion battery lithium-enriching technology and lithium ion battery prepared by the technology

The invention discloses a lithium ion battery lithium-enriching technology and a lithium ion battery prepared by the technology. The lithium-enriching technology comprises the following steps: evenly pre-mixing lithium powder and EC powder under a dry state at a temperature which is lower than the melting point of EC, then heating the mixture to a temperature which is higher than the melting point of EC to melt EC powder to evenly disperse lithium powder in the EC solvent so as to obtain lithium powder slurry; painting the obtain lithium powder slurry on at least one of the positive electrode sheet, the negative electrode sheet, or the diaphragm of a lithium ion battery, and then cooling to a temperature that is lower than the EC melting point so as to obtain a positive electrode sheet, negative electrode sheet and/or diaphragm containing a lithium-enriched surface layer. Compared to the prior art, the lithium-enriching technology has the advantages of simple preparation method, even dispersing effect, and no destruction on the surface protective layer of lithium powder during the dispersing process, moreover, the lithium-enriched layer does not to be dried after painting, and thus the phenomenon that lithium powder is oxidized and released into the air during the high temperature baking process is effectively avoided.
Owner:DONGGUAN AMPEREX TECH +1

Graphene-noble metal nanoparticle compound hydrogel and aerogel and preparing method and application thereof

The invention discloses a method for preparing graphene-noble metal inorganic nanoparticle compound hydrogel. The method comprises the steps of 1, evenly mixing oxidized graphene dispersion liquid, a noble metal compound and a reducing agent to obtain mixed liquid; 2, irradiating the mixed liquid with high-energy ray for irradiation reaction. The invention further provides compound hydrogel prepared with the method, and aerogel prepared after drying. According to the method for preparing the hydrogel, the in-situ reduction self-assembly method is adopted by means of the irradiation technique, operation is easy, and environment friendliness is realized; the compound aerogel is of a macroporous structure, noble metal is evenly dispersed and adsorbed on the surface of oxidized graphene, functions of graphene aerogel and functions of noble metal nanoparticles are combined, electric conductivity is high during organic solvent adsorption, corresponding electro-catalysis reaction is made feasible, and the method has great potential application value in organic reaction catalyzed synthesis including micromolecule electroanalysis and electro-catalysis, synthesis of petroleum organic intermediate and other fields.
Owner:SHANGHAI INST OF APPLIED PHYSICS - CHINESE ACAD OF SCI

Microbial fermented composite antibiotic-free feed containing natural antibacterial components

The present invention provides a microbial fermented composite antibiotic-free feed containing natural antibacterial components. The feed comprises a fermented product based on the united segmented fermentation of aerobic-anaerobic composite strains, composite natural antibacterial components, a non-plant source protein/polypeptide compound nutrient supplement agent, and an additive comprising atleast a soybean protein amino acid/polypeptide compound chelate. The composite strains comprises at least lactic acid bacteria, bacillus subtilis, yeast selected from candida utilis or saccharomyces cerevisiae, and enterococcus faecalis. The fermented product based on the united segmented fermentation is prepared by carrying out secondary fermentation on fermentation raw materials through the aerobic-anaerobic composite strains. The combination of the microbial fermented feed and the natural antibacterial components is beneficial to the balance of intestinal flora of animals, and can prevent the dysbacteriosis of digestive tracts, improve the immunity functions of animal organisms, reduce or replace the use of feed antibiotics, and significantly improve the digestion and absorption efficiency of the feed and the meat quality of animals.
Owner:JILIN QIAN KE LAI FEED TECH
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