Method for producing biodiesel by waste oil ester biological process
A biodiesel and biological process technology, which is applied in the preparation of biological raw materials, biofuels, and liquid hydrocarbon mixtures, etc., can solve the problems of toxic biocatalysts, high viscosity of the reaction system, and low methanol conversion rate, so as to avoid pollution and reduce Effect of reaction temperature, simplified raw material handling and product recovery process
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[0014] Mix the pretreated waste oil from the catering industry with methanol (the molar ratio of alcohol to oil is 1:1), and pump it into the first-stage fixed-bed enzyme reactor (diameter-to-height ratio 10×300mm, filled with 5g source) through a constant flow pump. The lipase of Candida antarctica) was transesterified at a flow rate of 6mL / h, and the effluent was allowed to stand for stratification, and the crude glycerin in the lower layer was separated, and the upper layer was mixed with methanol (alcohol to oil molar ratio 1:1) The second-stage fixed-bed enzyme reactor (diameter-to-height ratio 10×300mm, filled with 5g of lipase derived from Candida antarctica) was used for transesterification reaction at a flow rate of 6mL / h. Glycerol, supernatant and methanol (alcohol to oil molar ratio 1:1) were mixed and then entered into the third-stage fixed-bed enzyme reactor (diameter-height ratio 10-300mm, filled with 7g of lipase derived from Candida antarctica) for Transesterif...
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