Colorful and colorama rare earth luminous fibre and manufacturing method thereof
A technology of luminous fiber and colored light, which is applied in the fields of rayon manufacturing, fiber chemical characteristics, chemical instruments and methods, etc., can solve the problems of single color of luminous fiber, affect the development, utilization and popularization of luminous fiber, and achieve reduction of environmental pollution, The effect of improving traffic safety
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Embodiment 1
[0038] The manufacturing method of the color and color light rare earth luminous fiber of the present invention adopts the following process steps: the formula ratio is calculated by weight percentage:
[0039] 1. The manufacturing method of color photoluminescent light storage type luminescent base material:
[0040]1, get strontium nitrate: 2%, aluminum nitrate: 10%, europium oxide: 0.01%, dysprosium oxide: 0.01%, nitric acid solution (1mol / L): 67% and water: 20.98%, above-mentioned strontium nitrate, aluminum nitrate , europium oxide, dysprosium oxide, and nitric acid solution are dissolved in water at room temperature to prepare a metal nitrate aqueous solution; the percentage concentration of the metal nitrate aqueous solution: 5%;
[0041] 2. Take metal nitrate solution: 75%, add non-ionic surfactant 601A: 0.25%, stir at 85°C, gradually add 10% ammonia solution and 14.75% ammonium bicarbonate solution as precipitant, adjust After the pH value of the solution reaches 9, ...
Embodiment 2
[0053] Embodiment 2: The manufacturing method of the color and color light rare earth luminous fiber of the present invention adopts the following process steps: the formula ratio is calculated by weight percentage:
[0054] 1. The manufacturing method of color photoluminescent light storage type luminescent base material:
[0055] 1, get strontium nitrate: 5%, aluminum nitrate: 12%, europium oxide: 0.05%, dysprosium oxide: 0.05%, nitric acid solution (1mol / L): 70% and water: 12.9%, above-mentioned strontium nitrate, aluminum nitrate , europium oxide, dysprosium oxide, and nitric acid solution are dissolved in water at room temperature to prepare a metal nitrate aqueous solution; the concentration of the metal nitrate aqueous solution is 10%;
[0056] 2. Take metal nitrate solution: 80%, and add non-ionic surfactant 601A: 0.5%, stir at a temperature of 80°C, gradually add ammonia solution: 12% and ammonium bicarbonate solution (1:1): 7.5% as a precipitant, adjust the pH value...
Embodiment 3
[0063] Embodiment 3: The manufacturing method of the color and color light rare earth luminous fiber of the present invention adopts the following process steps: the formula ratio is calculated by weight percentage:
[0064] 1. The manufacturing method of color photoluminescent light storage type luminescent base material: polyamide sheet is selected as the raw material for spinning.
[0065] 1, get strontium nitrate: 7%, aluminum nitrate: 15%, europium oxide: 0.1%, dysprosium oxide: 0.1%, nitric acid solution (1mol / L): 65% and water: 12.8%, above-mentioned strontium nitrate, aluminum nitrate , europium oxide, dysprosium oxide, and nitric acid solution are dissolved in water at room temperature to prepare a metal nitrate aqueous solution; the concentration of the metal nitrate aqueous solution is 15%.
[0066] 2. Take metal nitrate solution: 85%, and add non-ionic surfactant AEO3: 0.5%, stir at a temperature of 90°C, gradually add ammonia solution: 7% and ammonium bicarbonate ...
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