Method for rapid medium-low temperature dry distillation of coal by using microwave

A low-temperature, rapid technology, applied in special forms of dry distillation, petroleum industry, coke oven, etc., can solve the problems of reducing the content of active components in gas, unfavorable comprehensive utilization of gas, and low coal pyrolysis speed, so as to improve the pyrolysis speed and effectively Conducive to comprehensive utilization and recycling, high heating efficiency

Inactive Publication Date: 2009-05-27
XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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Problems solved by technology

[0011] At present, domestic coal pyrolysis technology to produce blue coke (semi-coke) mainly includes coal solid heat carrier dry distillation polygeneration process, MRF pyrolysis process, STF pyrolysis technology, circulating fluidized bed thermoelectric technology based on fluidized bed pyrolysis Polygeneration process and heat and electricity polygeneration process based on moving bed. These methods can be summarized into two categories: external heat method and internal heat method. , although the quality of the gas produced is

Method used

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  • Method for rapid medium-low temperature dry distillation of coal by using microwave
  • Method for rapid medium-low temperature dry distillation of coal by using microwave

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Embodiment 1

[0024] Take 50g of Jurassic coal from a certain area in northern Shaanxi, the particle size is 200mm, and its composition is shown in Table 1. Put the Jurassic coal into a microwave-heated reactor with a microwave frequency of 0.3GHz to 300GHz, a final heating temperature of 700°C, and pyrolysis for 7min to 30min. After the tar was collected, the dry distillation gas was sampled and analyzed.

[0025] Table 1 Analysis results of raw coal

[0026]

[0027] Table 2 Analysis results of dry distillation gas

[0028] N 2 CO CH 4 CO 2 H 2 O 2 C 2 2.59 16.19 21.31 -- 59.76 0.15 2.24

[0029] Table 3 Analysis results of semi-coke (semi-coke)

[0030]

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Abstract

The invention discloses a method for carbonizing low-temperature coal of low metamorphic coal. The method adopts a microwave generation device as a heating source with the frequency of microwave of between 0.3 and 300 GHz; and the low metamorphic coal is heated to the a temperature of between 300 and 800 DEG C and is subjected to low-temperature carbonization to generate semi-coke, tar and coal gas. The method selects coal with shallow metamorphic degree as a raw material, utilizes a microwave radiation type heating mode to rapidly and selectively heat a coal material, depends on the dielectric property of the coal material to convert microwave energy and produce heat, utilizes the function of microwave activated molecules and achieves the aim of rapidly pyrolyzing the low metamorphic coal, thereby obtaining the semi-coke, tar and the low-temperature carbonization coal gas. The method has rapid coal pyrolyzing speed, can effectively improve the content of valuable compositions in the carbonation coal gas and is favorable for effective and comprehensive reclaiming of the coal gas.

Description

technical field [0001] The invention belongs to the technical field of coal pyrolysis, and relates to a method for low-metamorphic coal pyrolysis to produce semi-coke (semi-coke), coal tar and low-temperature dry distillation gas. It can also be used for coal drying, thermal power plant and boiler pretreatment before coal is put into the furnace, and extracts tar and valuable gas components in coal. Background technique [0002] With the increasing shortage of oil and natural gas resources, the further development and utilization of coal resources, especially the development of clean coal combustion and coal chemical technology has gradually become the focus of my country's energy development and utilization research. [0003] my country is a country rich in coal, short of oil, and low in natural gas. At present, my country's coal is mainly used for power generation, coking and power industries. Low-sulfur high-quality coal or coal types are usually required (such as gas co...

Claims

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Application Information

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IPC IPC(8): C10B53/00
Inventor 兰新哲赵西成马红周宋永辉李洪奇周军张秋利
Owner XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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