Method for modifying Kevlar fiber by treating nano sol through plasma

A Kevlar fiber, plasma technology, applied in the direction of fiber type, fiber treatment, physical treatment, etc., can solve the problem of no sol technology, no mention of coating polyolefin fibers, etc., to achieve molding processability and overall comprehensive performance Optimization, fast processing speed, the effect of causing environmental pollution

Inactive Publication Date: 2009-11-11
DONGHUA UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

At present, the existing patents do not use nano-materials to prepare sol technology, and there is no mention of using nano-sol technology to coat polyolefin fibers, especially the polyolefin fibers coated with nano-sols are then treated with plasma technology to Kevlar fibers. Methods of Surface Modification

Method used

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  • Method for modifying Kevlar fiber by treating nano sol through plasma
  • Method for modifying Kevlar fiber by treating nano sol through plasma
  • Method for modifying Kevlar fiber by treating nano sol through plasma

Examples

Experimental program
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Effect test

Embodiment 1

[0033] Helium plasma treatment of nano-silica sol coated Kevlar fiber

[0034] like figure 1 As shown, the Kevlar fiber 1 to be treated is immersed in a nano-silica sol with a concentration of 0.05% along the outer circle of the flower basket of the sol padding device 2, and the padding process is performed, and then the Kevlar fiber is introduced into the drying device 3. Dry at 70°C and collect the solvent, then the Kevlar fiber 1 is introduced into the plasma atmosphere area of ​​the plasma nozzle 4 for plasma surface modification treatment, the distance between the upper surface of the fiber bundle and the nozzle is 5MM, and the lower surface of the fiber bundle The distance from the nozzle is less than 20MM, the power is 40 watts, and the processing time is 2 seconds. The processed Kevlar fiber 1 is wound on the automatic winding machine 5, and the speed of the Kevlar fiber is adjusted by adjusting the speed of the winding shaft. . According to the needs of different pr...

Embodiment 2

[0037] Oxygen plasma treatment of nano-silica sol coated Kevlar fiber

[0038] like figure 1 As shown, the Kevlar fiber 1 to be treated is immersed in a nano-silica sol with a concentration of 0.05% along the outer circle of the flower basket of the sol padding device 2, and the padding process is performed, and then the Kevlar fiber is introduced into the drying device 3. Dry at 110°C and collect the solvent. Then the Kevlar fiber 1 is introduced into the plasma atmosphere area of ​​the plasma nozzle 4 for plasma surface modification treatment, the distance between the upper surface of the fiber bundle and the nozzle is 5MM, the distance between the lower surface of the fiber bundle and the nozzle is <20MM, the power is 40 watts, and the processing time is 2 Seconds, the processed Kevlar fiber 1 is wound online on the automatic winder 5, and the speed of the carbon fiber is adjusted by adjusting the speed of the winding shaft. According to the needs of different processing ...

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Abstract

The invention relates to a method for modifying Kevlar fiber by treating a nano sol through plasma, which comprises the following steps: (1) preparing inorganic nano particles into sol solution by ultrasonic oscillation technology; or (2) carrying out a hybridization reaction of precursor solution of organic-inorganic nano particles and the inorganic nano particles to prepare sol solution; (3) coating the sol solution on the surface of the Kevlar fiber; (4) drying the Kevlar fiber at a temperature of between 10 and 150 DEG C, collecting solvent, then introducing the Kevlar fiber in a plasma atmosphere area through a plasma generating device for surface modification treatment by the plasma; and finally, carrying out on-line winding of the treated Kevlar fiber in an automatic winding machine and adjusting the wiring speed of the Kevlar fiber by adjusting the speed range of a winding shaft. The combined performance between the Kevlar fiber treated by the method and the organic base materials is improved greatly; and the method has simple process, good treatment effect, low cost, difficult environmental pollution and reduction of the energy consumption.

Description

technical field [0001] The invention belongs to the field of preparation of Kevlar fiber surface modification, in particular to a method for plasma treatment of nano sol Kevlar fiber modification. Background technique [0002] Kevlar fiber is currently one of the most comprehensive and high-performance organic fibers produced on a large scale in the world. It has excellent mechanical properties, insulation properties, temperature resistance, and chemical resistance. It is also light in weight and can be used in manufacturing Structural materials, sheet insulation materials for motors, heat insulation materials, packaging materials, honeycomb materials, filter materials, high temperature resistant protective clothing and space suits, as reinforcement materials for high-performance composite materials, are widely used in aviation, aerospace, fields such as shipbuilding, automotive and construction. Therefore, it is of great significance to study and master the basic propertie...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M11/00D06M13/00D06M15/00D06M10/00C08J5/06D06M101/36
Inventor 张迎晨秦翊吴红艳邱夷平
Owner DONGHUA UNIV
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