Combined process for delayed coking and hydrotreating
A hydrotreating and delayed coking technology, applied in the combined process field, can solve the problems of heavy distillation range of coking wax oil, complex fractionation tower process, high aromatics content, etc., achieve process optimization, ensure long-term operation, reduce coke yield and The effect of gas yield
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[0031] Example 1
[0032] The feedstock oil used in Example 1 is high-sulfur slag reduction, and its properties are listed in Table 1.
[0033] The reaction conditions for delayed coking are that the temperature at the outlet of the heating furnace is 500°C, the pressure at the top of the coke tower is 0.17MPa, and the circulation ratio is 0. The oil and gas at the top of the coke tower are separated into gas and liquid components after heat exchange and cooling. The liquid components of the whole coking fraction (including naphtha, diesel and wax oil fractions) are pressurized and carried out with hydrogen in a reactor under hydrotreating conditions, and the reactor is filled with a hydrotreating agent and a hydrotreating catalyst The ratio of the two is 15:85. The specific reaction conditions, product distribution and product properties are listed in Table 2 to Table 4 respectively.
[0034] It can be seen from Table 2 that the yield of coking liquid products is 63.7% by weight. I...
Example Embodiment
[0035] Example 2
[0036] The feedstock oil used in Example 2 is acid-containing cycloalkyl residue reduction, and its properties are listed in Table 5.
[0037] The reaction conditions for delayed coking are that the temperature at the outlet of the heating furnace is 500°C, the pressure at the top of the coke tower is 0.17MPa, and the circulation ratio is 0. The oil and gas at the top of the coke tower are separated into gas and liquid components after heat exchange and cooling. The liquid components of the whole coking fraction (including naphtha, diesel and wax oil fractions) are pressurized and carried out with hydrogen in a reactor under hydrotreating conditions, and the reactor is filled with a hydrotreating agent and a hydrotreating catalyst The filling ratio is 15:85. The specific reaction conditions, product distribution and product properties are listed in Table 6 to Table 8.
[0038] It can be seen from Table 6 that the yield of coking liquid products is 71.23% by weight...
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