Conductive ink and preparation method thereof
A conductive ink, mass percentage technology, applied in the direction of ink, household utensils, applications, etc., can solve the problems that high-end fields cannot be applied, high-conductivity fields cannot be applied, and slurry square resistance increases, so as to achieve good compactness and good conductivity , Reduce the effect of slurry square resistance
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preparation example Construction
[0028] The preparation method of above-mentioned conductive ink, comprises the following steps:
[0029] (1) Organic carrier A: weighing 65-75% of diethyl adipate or ethylene glycol butyl ether acetate and 25-35% of polyester resin or acrylic acid One of the resin-like, high-speed stirring in the water bath, so that the resin is completely dissolved in the solvent;
[0030] (2) Organic carrier B: Weigh one of 62-77% 1,4-butyrolactone or terpineol and 22-38% vinyl acetate resin in a water bath at high speed Stir to completely dissolve the resin in the solvent, add a coupling agent with a mass percentage of 0.05%-1%, and make it after high-speed stirring;
[0031] (3) Preparation of carbon silver paste:
[0032] Weigh the proportioning amount of carbon powder and organic carrier A, mix thoroughly, and then use a three-roll mill to grind and disperse to form a uniform mixed phase to obtain carbon slurry;
[0033] Weigh a piece of silver, nickel powder and organic carrier B, mi...
Embodiment 1
[0043] Organic carrier A:
[0044] Weigh 101.35 grams of diethyl adipate and 43.5 grams of polyester resin, place them in a water bath at 70-100°C, and stir at high speed for 2 hours to completely dissolve the polyester resin in diethyl adipate.
[0045] Organic carrier B:
[0046] Weigh 202.70 grams of 1,4-butyrolactone and 87.0 grams of chloroacetic resin, mix 1,4-butyrolactone and chloroacetic resin, and place in a water bath at 70-100°C, stir at a high speed for 2 hours to make Vinyl resin is completely soluble in 1,4-butyrolactone. Add 0.15 g of silane coupling agent KH-551 and stir at high speed for 20 minutes.
[0047] Weigh the material according to the following ratios
[0048]
[0049] The carbon powder and the organic carrier A are weighed and mixed thoroughly, and then the three-roll mill is used to grind and disperse 3 to 5 times to form a uniform mixed phase to obtain a carbon slurry.
[0050] The silver flakes, nickel powder, and organic vehicle B were we...
Embodiment 2
[0052] Organic carrier A:
[0053] Weigh 101.35 grams of ethylene glycol butyl ether acetate and 43.5 grams of polyester resin, place them in a water bath at 70-100 ° C, and stir at high speed for 2 hours to completely dissolve the polyester resin in ethylene glycol butyl ether acetate .
[0054] Organic carrier B:
[0055] Weigh 202.70 grams of 1,4-butyrolactone and 87.0 grams of chloroacetic resin, mix 1,4-butyrolactone and chloroacetic resin, and place in a water bath at 70-100°C, stir at a high speed for 2 hours to make Vinyl resin is completely soluble in 1,4-butyrolactone. Add 0.15 g of silane coupling agent KH-551 and stir at high speed for 20 minutes.
[0056] Weigh the material according to the following ratios
[0057]
[0058] The carbon powder and the organic carrier A are weighed and mixed thoroughly, and then the three-roll mill is used to grind and disperse 3 to 5 times to form a uniform mixed phase to obtain a carbon slurry.
[0059] The silver flakes, ni...
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