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Method for preparing high-temperature resistant essence microcapsules

A flavor microcapsule and warming aroma technology, which is applied in the field of preparation of high-temperature-resistant flavor microcapsules, can solve the problems of affecting the use effect of microcapsules, production of high-temperature-resistant microcapsules, and inappropriateness, so as to achieve protection of flavor components and excellent slow-release performance , Consolidate the effect of protection

Inactive Publication Date: 2010-05-19
SHAANXI UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the microcapsules prepared by the spray drying method in the industry at present have the disadvantage that the microcapsule wall material is water-soluble. In the process of making baked products, the microcapsule wall material is usually dissolved and ruptured due to the need for ingredients in water, and the essence of the core material is released. , at high temperature, the essence degrades and loses its aroma-giving effect on baked products, which seriously affects its use as microcapsules. Therefore, the simple spray drying method is not suitable for directly preparing microcapsule products with high temperature resistance.
In order to prepare high-temperature-resistant flavor microcapsules, the premise is that the wall material does not dissolve in the production of baked food. At present, the method suitable for embedding liquid core materials to make water-insoluble wall material microcapsules is mainly the complex coacervation method, but this method The curing agents used in the production of microcapsule products are chemical reagents such as formaldehyde and glutaraldehyde. These chemical reagents are toxic to the human body and are prohibited in the food industry. Therefore, this method cannot be used to directly produce high-temperature resistant microcapsules.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] 1) Gelatin and gum arabic of the same quality are respectively configured into a gelatin aqueous solution and a gum arabic aqueous solution with a mass concentration of 3%, and then homogeneous emulsification is carried out after adding gelatin and gum arabic total mass 30% oil-soluble essence in the gum arabic aqueous solution , and then mix the emulsified solution with the gelatin aqueous solution at 40°C to obtain an emulsion;

[0013] 2) Regulating the pH of the emulsion with 10% edible acetic acid with a mass concentration of 4.15;

[0014] 3) Curing: Dissolve gelatin and Gum Arabic solidifying agent transglutaminase with a total mass of 1.2% in water, activate it at 45°C for 10 minutes, mix it with an emulsion with a pH of 4.15, and cure it for 60 minutes at a stirring speed of 60 r / min. The mass ratio of said transglutaminase to water is 1: 10;

[0015] 4) Incubate the solidified emulsion at 5°C for 30 minutes, then filter, discard the supernatant, and collect t...

Embodiment 2

[0018] 1) Gelatin and gum arabic of the same quality are respectively configured into a gelatin aqueous solution and a gum arabic aqueous solution with a mass concentration of 3%, and then homogeneous emulsification is carried out after adding gelatin and gum arabic total mass 50% oil-soluble essence in the gum arabic aqueous solution , and then mix the emulsified solution with the gelatin aqueous solution at 45°C to obtain an emulsion;

[0019] 2) adjusting the pH of the emulsion to 4.16 with a mass concentration of 10% edible acetic acid;

[0020] 3) Curing: take 1% of the total mass of gelatin and gum arabic as a curing agent, transglutaminase, dissolve it in water, activate it at 45°C for 10 minutes, mix it with an emulsion with a pH of 4.16, and cure it for 60 minutes at a stirring speed of 60r / min. The mass ratio of said transglutaminase to water is 1: 10;

[0021] 4) Incubate the solidified emulsion at 3°C ​​for 30 minutes, then filter, discard the supernatant, and col...

Embodiment 3

[0024] 1) Gelatin and gum acacia of the same quality are respectively configured into a gelatin aqueous solution and a gum arabic aqueous solution with a mass concentration of 3%, and then homogeneous emulsification is carried out after adding gelatin and gum arabic total mass 40% oil-soluble essence in the gum arabic aqueous solution , and then mix the emulsified solution with the gelatin aqueous solution at 42°C to obtain an emulsion;

[0025] 2) Regulating the pH of the emulsion with 10% edible acetic acid with a mass concentration of 4.17;

[0026] 3) Curing: take gelatin and gum arabic as a curing agent transglutaminase with a total mass of 1.1%, dissolve it in water, activate it at 45°C for 10 minutes, mix it with an emulsion with a pH of 4.17, and cure it for 60 minutes at a stirring speed of 60 r / min. The mass ratio of said transglutaminase to water is 1: 10;

[0027] 4) Incubate the solidified emulsion at 1°C for 30 minutes, then filter, discard the supernatant, and ...

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Abstract

The invention discloses a method for preparing high-temperature resistant essence microcapsules, which comprises the following steps: preparing aqueous solution of gelatin and aqueous solution of Arabic gum by gelatin and Arabic gum respectively, then adding oil-soluble essence into the aqueous solution of Arabic gum and performing homogenization and emulsification on the solution, and uniformly mixing the emulsified solution and the aqueous solution of gelatin to obtain emulsified liquid; adjusting the pH of the emulsified liquid to 4.15-4.17 by using edible acetic acid; dissolving a curing agent glutamine transaminase in water, and then mixing solution of the curing agent and the emulsified liquid to perform curing; filtering the cured emulsified liquid, discarding the supernate, and collecting the sediment; dissolving a wall material obtained by mixing Arabic gum, malt dextrin, glucose and isolated soy protein in the water, then adding the collected sediment into the solution of wall material to be uniformly mixed, and preparing the mixture into the high-temperature resistant essence microcapsules by adopting a spray drying method. The method prepares the oil-soluble essence into the microcapsules so as to keep the primary fragrance of the essence and ensure the using effect in high-temperature processing.

Description

technical field [0001] The invention relates to a preparation method of microcapsules, in particular to a preparation method of high-temperature-resistant essence microcapsules. Background technique [0002] With the improvement of people's living standards and the rapid development of the food industry, the application of food flavors is becoming more and more extensive. In the process of making baked food, since the processing temperature is often above 200°C, the flavor components in the product will be destroyed because they cannot withstand the high temperature, resulting in insufficient flavor of the product. Therefore, in processing, it is particularly necessary to have a flavor that can withstand high temperatures to add flavor to baked goods. Making the essence into a microcapsule form should be able to protect the essence and reduce loss. However, the microcapsules prepared by the spray drying method in industry at present have the disadvantage that the microcaps...

Claims

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Application Information

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IPC IPC(8): B01J13/02A23P1/04A23L1/22A23L27/00A23P10/30
Inventor 陈雪峰刘楠楠孟继生范娜
Owner SHAANXI UNIV OF SCI & TECH
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