Poly-arylene ether nitrile composite material, poly-arylene ether nitrile bar and preparation method thereof
A technology for poly(arylene ether nitrile) and composite materials is applied in the fields of poly(arylene ether nitrile) rods and their preparation, and poly(arylene ether nitrile) composite materials. Effect
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[0042] Example 1
[0043] Take 5640 grams of polyarylene ether nitrile, 180 grams of phthalonitrile prepolymer, 120 grams of graphite and 60 grams of silicon carbide whiskers, blend them uniformly and add them to the single-screw extruder to control the extrusion of the single-screw extruder. The outlet temperature is 330-350℃, and they are plasticized in the screw to obtain molten materials. The molten material is extruded into the die through the filter plate through the head of the extruder, and then directly enters the cooling sizing sleeve. The length of the sizing sleeve is 120mm and the diameter is D42mm. Under the combined action of the back pressure rod of the traction device and the extruder, the polyarylene ether nitrile melt moves forward at a constant speed, and is cooled and shaped by the sizing sleeve to obtain a diameter of D41mm? mm polyarylene ether nitrile rod.
[0044] After cutting the polyarylene ether nitrile bar, it is put into a box annealing furnace for...
Example Embodiment
[0051] Example 2
[0052] As in Example 1, just change the formula to 3780 grams of polyarylene ether nitrile, 300 grams of phthalonitrile prepolymer, 120 grams of graphite and 1800 grams of glass fiber, and then add them to the single screw extruder. According to the method and process, the polyaryl ether nitrile rod is obtained.
[0053] The roundness of the bar prepared in this example was studied. Therefore, the diameter of the bar was measured at 5 different points on the cross section of the prepared bar. The results are as follows:
[0054] Table 3 Diameter data of polyarylene ether nitrile rod prepared in Example 1
[0055]
[0056] Table 4 Performance data of polyarylene ether nitrile rods prepared in Example 1
[0057]
[0058] It can be seen from Tables 3 and 4 that the prepared polyarylene ether nitrile rods have uniform cross-sections and high mechanical strength and heat resistance.
Example Embodiment
[0059] Example 3
[0060] As in Example 1, just change the formula to 4380 grams of polyarylene ether nitrile, 300 grams of phthalonitrile prepolymer, 120 grams of polytetrafluoroethylene and 1200 grams of carbon fiber, and then add them to the single screw extruder. , The same method and process, to obtain polyaryl ether nitrile rod.
[0061] The roundness of the bar prepared in this example was studied. Therefore, the diameter of the bar was measured at 5 different points on the cross section of the prepared bar. The results are as follows:
[0062] Table 5 Diameter data of polyarylene ether nitrile rods
[0063]
[0064] Table 6 Performance data of polyarylene ether nitrile rods
[0065]
[0066] It can be seen from Tables 5 and 6 that the prepared polyarylene ether nitrile rods have uniform cross-sections and high mechanical strength and heat resistance.
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