Real-time fluorescence PCR primer for perkinsosis detection and probe
A real-time fluorescence, piquing worm technology, applied in the field of epidemiology and food hygiene detection, can solve the problems of low sensitivity, low detection sensitivity, long time consumption, etc., and achieve the effect of strong specificity
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Embodiment 1
[0026] Embodiment 1 Piedia FTM culture method
[0027] 1. Sample pretreatment
[0028] Take shellfish samples that reach a certain statistical significance, place them in a sterilized mortar, measure the length, width, and thickness, discard the shells, weigh the net weight of the tissue with a balance, and place it in a sterilized research mortar. Bowl, grind to 0.1mm 3 about.
[0029] 2. Incubation of samples
[0030] Place the samples in sterilized centrifuge tubes containing 5mL of FTM medium, add 250μL of 2.5% chloramphenicol and shake well, cover the liquid with 1mL of 1% nystatin, close the lid, and place in a dark room at 22-24°C Culture 5-7d.
[0031] 3. Purification of samples
[0032] Centrifuge the cultured sample at 4000r / min for 10min, discard the supernatant, add 6mL of 2mol / L NaOH, vortex and mix well, and place it in an oven at 55°C for overnight digestion. Centrifuge at 4000r / min for 10min, discard the supernatant, add 2mL ddH 2 O wash, centrifuge at 4...
Embodiment 2
[0037] Preparation of embodiment 2 primers and probes
[0038] 1 Design and synthesis of primers and probes
[0039] Select the relatively conserved ITS-2 region in the ribosomal DNA sequence of Pietia worm, and design it with the software Beacon Designer7.0. The primer pair was determined to be the specific primer pair of Pijenia by online sequence BLAST analysis. And set a specific fluorescent TaqMan probe in the amplification region of the primer pair.
[0040] The primer sequences used in this example are:
[0041] Upstream primer: (forward): 5'-GAAGAATGGCGTGATCAAGGAAC-3';
[0042] Downstream primer: (reverse): 5'-TGCAAGGCTATAATCTCGTATTGTAG-3', the length of the amplified product is 126bp;
[0043] The sequence of the probe is: 5'FAM-CAACACAGTCGGACTTGCGAGCATCCAAFAMRA-3', the 5' end of the probe is marked with a fluorescent reporter group 6-carboxyfluorescein (6-carboxyfluorescein, FAM), and the 3' end is marked with a fluorescence quencher Killing group 6-carboxytetra...
Embodiment 3
[0046] Embodiment 3 Establishment of the detection method of Piedia worm fluorescent PCR
[0047] 1 Genomic DNA extraction from diseased tissue
[0048] Take 25 mg of the gill tissue of the Philippine clam that was infected with Piechinia by FTM culture, extract the genomic DNA according to the instructions of the kit (QIAGEN, 69506), and store it at -20°C for future use.
[0049] 2PCR amplification of the target gene
[0050] Using primers to use the genomic DNA of the diseased tissue as a template, the above-mentioned extracted DNA was amplified by PCR using the Piedia specific primers AF and AR published by Liang Yubo (2005). The primer sequences are: AF: 5'-CCGCTTTGTTTGGMTCCC-3'; AR: 5'-ACATCAGGCCTTCTAATGATG-3. PCR reaction system reference: 0.5 μL of primer AF (10 μmol / L), 0.5 μL of primer AR (10 μmol / L), 0.5 μL of fluorescent probe (10 μmol / L), 10×buffer (containing Mg 2+ ) 2.5 μL, dNTP (2.5mmol / L) 2 μL, rTaq DNA polymerase (5U / μL) 0.5 μL, sterilized ddH 2 O suppleme...
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