Soy protein oligopeptide, and preparation method and use thereof
A soybean oligopeptide and soybean protein technology, which is applied in the field of enzyme catalysis, can solve the problems of inability to completely eliminate bitterness and odor, low degree of automation and complex process.
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[0073] The present invention provides a preparation method of soybean protein oligopeptide, which comprises the steps of: adding compound enzyme A to hydrolyze the raw material after processing, the hydrolysate is subjected to microfiltration, and then passed through D315 and 335 resin for desalting and decolorization, and finally making soybeans Protein oligopeptides.
[0074] In a preferred embodiment of the present invention, based on the total weight of the solids, the added amount of the composite enzyme A is added at 1-3 w / w% of the solids content.
[0075] In a preferred embodiment of the present invention, the hydrolysis used is at 55°C-65°C and pH 8-9 for 8-12 hours; more preferably, it is incubated at 75-85°C for 30 minutes.
[0076] In another preferred embodiment of the present invention, the raw material of the method for preparing soy protein oligopeptides is soy protein isolate, which includes the following steps:
[0077] 1) Raw material pretreatment: mix the soybean p...
Embodiment 1
[0120] Hydrolysis of Soy Protein by Complex Enzyme A
[0121] Within the range of 45-85w / w%, gradually adjust the percentage concentration of keratinase in the complex enzyme A, and then follow the steps 1) to 2) described in Example 2(1), or Example 2(2) Step 1) to step 4) described in Example 2(3), or step 1) to step 5) described in Example 2(3), implement the hydrolysis of soybean protein by complex enzyme A (the amount of complex enzyme A is 2w of the amount of raw materials / w% added), after the hydrolysis, take 5ml of the enzymatic hydrolysate and centrifuge at 12000rpm for 5 minutes, take the supernatant and use the Folin-phenol method to determine the soluble protein content, and calculate the degree of hydrolysis DH according to the following formula:
[0122] DH ( % ) = ( N 2 - N 1 ) X V N 0 X 100
[0123] Where: N 2 --The soluble protein content of the enzymolysis solution after enzymolysis reaction, mg / mL;
[0124] ...
Embodiment 2
[0134] Preparation of soybean protein oligopeptides
[0135] (1) Using soybean protein isolate as raw material
[0136] Using soybean protein isolate as raw material, the preparation of soybean protein oligopeptides is carried out according to the following steps, and the process flow is as follows: image 3 Shown.
[0137] 1) Raw material pretreatment: mix the soy protein isolate with water (m / v) according to the solid-liquid ratio 1:3-1:9, adjust the pH to between 5-6, heat up to 30℃-40℃, and then Incubate for 30 minutes under the conditions, and then grind the mixture into an emulsion through colloid grinding;
[0138] 2) Enzymatic hydrolysis: add the emulsion to the reaction tank, adjust the pH to 8-9, heat up to 55℃-65℃, add compound enzyme A (m / m) according to 1%-3% of the solid content, mix After homogenization, hydrolyze under these conditions for 8-12 hours, then quickly increase the temperature to 75℃-85℃ and keep it for 30 minutes;
[0139] 3) Separation: reduce the tempera...
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