Method for preparing powdery amphoteric guar gum derivative
A technology of amphoteric guar gum and derivatives, which is applied in the directions of reinforcing agent addition, paper, textile and papermaking, etc., can solve the problems of difficult post-processing, low product substitution, and the effect is not as good as high substitution, and achieves high substitution and lower The effect of improving cost and burst resistance index
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Embodiment 1
[0017] Dissolve 2g of alkali in a mixture of 20ml of water and 3.5ml of ethanol, spray it into 50g of guar collagen powder and stir for 0.5h. The guar collagen powder was fully alkalized, and 10 g of 3-chloro-2-hydroxypropyltrimethylammonium chloride was added within 0.5 h under stirring conditions, and the stirring was continued for 0.5 h. Then the temperature was raised to 65°C, and after 30 min of heat preservation, 8 g of sodium chloroacetate was added within 0.5 h under stirring conditions, and the stirring was continued for 0.5 h. The reaction temperature was maintained at 70°C, and after 4 hours of reaction, the temperature was lowered, and the pH value was adjusted to 7 with hydrochloric acid. The crude product is soaked in 95% ethanol, filtered, washed, and vacuum-dried to obtain amphoteric guar gum in the form of light yellow powder with high degree of substitution. The main technical parameters of the product are: nitrogen content 2.10%, cation substitution degree ...
Embodiment 2
[0019] Dissolve 2g of alkali in a mixture of 15ml of water and 3ml of ethanol, spray it into 50g of guar collagen powder and stir for 0.5h. The guar collagen powder was fully alkalized, and 7.5 g of 3-chloro-2-hydroxypropyltrimethylammonium chloride was added within 0.5 h under stirring conditions, and the stirring was continued for 0.5 h. Then the temperature was raised to 65°C, and after 30 min of heat preservation, 5 g of sodium chloroacetate was added within 0.5 h under stirring conditions, and the stirring was continued for 0.5 h. The reaction temperature was maintained at 75°C, and after 4 hours of reaction, the temperature was lowered, and the pH value was adjusted to 7 with acetic acid. The crude product is soaked in 95% ethanol, filtered, washed, and vacuum-dried to obtain amphoteric guar gum in the form of light yellow powder with high degree of substitution. The main technical parameters of the product are: nitrogen content 1.80%, cation substitution degree 0.258, ...
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