Preparation process of nano powder modified and reinforced die steels
A nano-powder and preparation technology, which is applied in the field of mold steel, can solve the problems of high melting temperature of mold steel, difficulty in quality assurance, and poor quality stability of alloy steel, etc., to improve wetting performance, wear resistance, and dispersion degree of effect
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Embodiment 1
[0043] Adding nanoparticles to H13 hot work die steel for modification and strengthening. The chemical composition of H13 hot work die steel is C 0.31~0.45, Cr4.75~5.5, Mo1.10~1.75, Si0.81~1.20, V0.80~1.20, Mn<0.40, and the weight is 1000kg. The material of the nanoparticles is TiN, the particle size is 60nm, and the added amount is 0.5% by weight. The preparation process is:
[0044] 1. Nanoparticle pretreatment process:
[0045] The nanoparticles are pretreated before being added to increase the wettability of the nanoparticles and the steel matrix. The pretreatment process is:
[0046] a. Pour 25000ml of analytical pure ethanol into the container according to the ratio of nanoparticle mixed powder and ethanol to 1g / 5ml, put 5kg of TiN nanoparticles with a particle size of 60nm into the container of analytical pure ethanol, Stir and fully moisten;
[0047] c. Weigh the above-mentioned TiN nanoparticles after pretreatment and the iron powder with a particle size of 200 me...
Embodiment 2
[0058] in Cr 12 Adding nanoparticles to MoV cold work die steel for modification and strengthening. Cr 12 The chemical composition of MoV cold work die steel is C1.45~1.70, Cr4.75~5.5, Mo0.40~0.60, Si<0.40, V0.15~0.30, Mn<0.40, and the weight is 1000kg. The material of the nanoparticles is WC, the size of the particles is 100nm, and the added amount is 0.6% by weight.
[0059] 1. Nanoparticle pretreatment process:
[0060] a. Pour 42000ml of analytical pure ethanol into the container according to the ratio of nanoparticle mixed powder and ethanol to 1g / 7ml, put 6kg of WC nanoparticles with a particle size of 100nm into the container of analytical pure ethanol, Stir and fully moisten;
[0061] c. The above-mentioned WC nanoparticles after pretreatment and the iron powder with a particle size of 200 meshes for pre-diffusion are weighed according to the ratio of 1:1.5 by weight, and put into a stirring ball mill to stir and mix evenly, which will account for the volume of the a...
Embodiment 3
[0066] at W 6 Mo 5 Cr 4 V 2 Adding nanoparticles to high-speed steel for modification and strengthening. W 6 Mo 5 Cr 4 V 2 The chemical composition of high-speed steel is C0.80~0.90, Cr3.80~4.40, W4.50~5.50, Mo5.50~6.75, Si<0.40, Mn<0.40, V1.75~2.25, and the weight is 1000kg. The material of the nanoparticles is TiC, the particle size is 80nm, and the added amount is 0.8% by weight.
[0067] 1. Nanoparticle pretreatment process:
[0068] The nanoparticles are pretreated before being added to increase the wettability of the nanoparticles and the steel matrix. The pretreatment process is:
[0069] a. Pour 48000ml of analytical pure ethanol into the container according to the ratio of nanoparticle mixed powder and ethanol to 1g / 6ml, put 8kg of TiC nanoparticles with a particle size of 80nm into the container of analytical pure ethanol, Stir and fully moisten;
[0070] c. Weigh the above-mentioned TiC nanoparticles after pretreatment and the iron powder with a particle ...
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