Method for preparing small expended and vitrified ball with reinforcing layer coated on surface

A technology of expanded vitrified microbeads and surface coating, which is applied in the field of preparation of expanded vitrified microbeads, can solve the problems of improving the strength of expanded vitrified microbeads, etc., and achieves the effects of improving comprehensive performance, increasing strength and reducing water absorption.

Inactive Publication Date: 2011-02-16
WUHAN TEXTILE UNIV
View PDF6 Cites 25 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Chinese patent application number 200710031860.1, published on May 28, 2008, the title of the invention patent is "A Modified Vitrified Microbead Thermal Insulation Mortar and Its Preparation Method". Low-quality vitrified microbeads, and then use modified vitrified microbeads to prepare modified vitrified microbead thermal insulation mortar. , but did not improve the strength of expanded vitrified beads
So far, no reports have been found on the surface coating of thermosetting resins to enhance the expansion of vitrified microbeads

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Get 25g ammonium chloride solid, be mixed with concentration and be 1% ammonium chloride aqueous solution. Take 3.75g of urea-formaldehyde resin, add 8ml of 1% ammonium chloride solution, and add 22ml of deionized water, and mix them uniformly to obtain a urea-formaldehyde resin / ammonium chloride solution.

[0024] Take 75g of expanded vitrified microbeads, and then spray the above prepared urea-formaldehyde resin / ammonium chloride solution evenly on the surface of the expanded vitrified microbeads using a spray facility.

[0025] The expanded vitrified microspheres whose surface is coated with the reinforcing liquid are cured at room temperature.

[0026] Put the expanded vitrified microbeads coated with a reinforcing layer on the surface obtained after curing into a drying box, and dry them for 2 hours at a temperature of 110° C. to obtain expanded vitrified microbeads with a urea-formaldehyde resin surface coated reinforcing layer, The cylinder compressive strength ...

Embodiment 2

[0028] Get 25g ammonium chloride solid, be mixed with the ammonium chloride solution that concentration is 1%. Take 50g of urea-formaldehyde resin, add 100ml of 1% ammonium chloride solution, and add 150ml of deionized water, and mix them uniformly to obtain a urea-formaldehyde resin / ammonium chloride solution.

[0029] Take 75g of expanded vitrified microbeads, and then spray the above prepared urea-formaldehyde resin / ammonium chloride solution evenly on the surface of the expanded vitrified microbeads using a spray facility.

[0030] The expanded vitrified microspheres whose surface is coated with the reinforcing liquid are cured at room temperature.

[0031]Put the expanded vitrified microbeads coated with a reinforcing layer on the surface obtained after curing into a drying box, and dry them for 2 hours at a temperature of 110° C. to obtain expanded vitrified microbeads with a urea-formaldehyde resin surface coated reinforcing layer, The cylinder compressive strength is ...

Embodiment 3

[0033] Get 50g ammonium chloride solid, be mixed with concentration and be 1% ammonium chloride solution. Take 150 g of urea-formaldehyde resin, add 300 ml of 1% ammonium chloride aqueous solution, and add 450 ml of deionized water, and stir it evenly to obtain a urea-formaldehyde resin / ammonium chloride solution.

[0034] Take 75g of expanded vitrified microbeads, and then spray the above prepared urea-formaldehyde resin / ammonium chloride solution evenly on the surface of the expanded vitrified microbeads using a spray facility.

[0035] The expanded vitrified microspheres whose surface is coated with the reinforcing liquid are cured at room temperature.

[0036] Put the expanded vitrified microbeads coated with a reinforcing layer on the surface obtained after curing into a drying box, and dry them for 2 hours at a temperature of 110° C. to obtain expanded vitrified microbeads with a urea-formaldehyde resin surface coated reinforcing layer, The cylinder compressive strength...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
particle sizeaaaaaaaaaa
densityaaaaaaaaaa
melting pointaaaaaaaaaa
Login to view more

Abstract

The invention relates to a method for preparing a small expended and vitrified ball with a reinforcing layer coated on the surface. By combining the advantages of the small expended and vitrified ball and a thermosetting polymer material, the small expended and vitrified ball with the reinforcing layer coated on the surface is prepared by forming an insoluble and infusible high molecular protective film on the surface of the small expended and vitrified ball through the crosslinking and solidification of thermosetting resin. The strength and the heat-preservation and heat-insulating performance of the small expended and vitrified ball with the reinforcing layer coated on the surface are improved, the problems that the small expended and vitrified ball is easy to crack in use and the like are reduced, and meanwhile, the water absorption rate of the small expended and vitrified ball is reduced greatly. The method has the advantages that the preparation process is simple, the small expended and vitrified ball is easy to control and the like. The small expended and vitrified ball with the reinforcing layer coated on the surface can be used as heat-preservation light mortar and a plaster material, a heat-preservation and heat-insulating layer in oil cans, liquefied gas storage tanks and industrial gas storage tanks and a raw material of a light high-grade refractory material.

Description

technical field [0001] The invention relates to a method for preparing expanded vitrified microbeads with a surface coating reinforcement layer, belonging to the field of polymer composite materials. Background technique [0002] With the increasingly sharp contradiction between economic development and resources and environment, people's awareness of environmental protection is increasing, and new materials for energy saving and environmental protection have become a hot research topic. In terms of building energy-saving materials, expanded vitrified microbeads have entered people's field of vision due to their advantages in environmental protection, energy saving, and heat preservation. A new type of inorganic lightweight thermal insulation material. Expandable vitrified microbeads are a kind of acidic vitreous lava minerals. After crushing, screening, high-temperature instantaneous combustion and expansion vitrification, they are spherical fine-diameter particles with po...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C04B20/10
Inventor 王罗新蔡静平刘伟华罗淑湘甘厚磊易长海邹汉涛
Owner WUHAN TEXTILE UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products