Microemulsion preparation taking rosin-based vegetable oil as solvent and preparation method thereof

A technology of turpentine-based vegetable oil and emulsion preparation, which is applied in the fields of botanical equipment and methods, plant growth regulators, animal repellents, etc. Odor, excellent spreading permeability, effect of improving stability over time

Active Publication Date: 2011-03-16
FUJIAN NUODE BIOTECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Compared with emulsifiable concentrates, microemulsions replace most of the organic solvents with water, and the safety performance has been greatly improved, but it still needs to use a certain amount of aromatic hydrocarbons and other non-environmentally friendly organic solvents or polar solvents to dissolve and disperse the active ingredients of pesticides, and The emulsifiers used are usually not biodegradable, so there are certain unsafe hazards to the environment and people, which need to be improved

Method used

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  • Microemulsion preparation taking rosin-based vegetable oil as solvent and preparation method thereof
  • Microemulsion preparation taking rosin-based vegetable oil as solvent and preparation method thereof
  • Microemulsion preparation taking rosin-based vegetable oil as solvent and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0040] Weigh 18kg of avermectin, 100kg of rosin-based vegetable oil, 100kg of ethanol, 40kg of polyoxyethylene polyoxypropylene block copolymer, 30kg of C12-14 polyoxyethylene ether phosphate, and 30kg of linear calcium dodecylbenzenesulfonate 1 kg of methylpolysiloxane was added to the reactor, and it was sheared and dispersed evenly at 2000rpm / min; 681kg of deionized water was added, and it was sheared at a high speed of 5000rpm / min for 60min to form a 1000kg abamectin microemulsion preparation.

Embodiment 2

[0050] Weigh 50kg of avermectin, 150kg of rosin-based vegetable oil, 100kg of N-octylpyrrolidone, 50kg of polyoxyethylene polyoxypropylene block copolymer, 40kg of C12-14 polyoxyethylene ether phosphate, linear dodecylbenzene Add 40kg of calcium sulfonate and 1kg of methylpolysiloxane into the reactor, and shear and disperse evenly at 5000rpm / min; add 569kg of deionized water, and shear at 8000rpm / min for 20min to form 1000kg of abamectin microemulsion preparation.

Embodiment 3

[0052] Weigh 25kg of lambda-cyhalothrin, 60kg of turpentine-based vegetable oil, 20kg of ethylene glycol, 20kg of polyoxyethylene polyoxypropylene block copolymer, 20kg of fatty alcohol polyoxyethylene ether phosphate, linear dodecylbenzenesulfonate Add 25kg of acid amine and 1kg of methyl polysiloxane into the reaction kettle, and shear and disperse evenly at 3000rpm / min; add 829kg of deionized water, and shear at 5000rpm / min for 20min to form 1000kg of efficient cyhalothrin microemulsion preparation.

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Abstract

The invention provides a microemulsion preparation taking rosin-based vegetable oil as a solvent and a preparation method thereof, and relates to a pesticide preparation. The microemulsion preparation consists of the following raw materials in percentage by mass: 0.5 to 30 percent of pesticide active ingredients, 55 to 20 percent of emulsifier, 0 to 8 percent of cosolvent, 0.1 to 0.3 percent of defoamer, 1 to 30 percent of rosin-based vegetable oil, and the balance of water. The preparation method comprises the following steps of: adding the pesticide active ingredients, the rosin-based vegetable oil, the cosolvent, emulsifier and the defoamer into a reaction kettle, performing cutting and uniform dispersion at 2,000 to 5,000 rpm/min, and adding the balance of water into the mixture for high-speed cutting to obtain the microemulsion preparation taking the rosin-based vegetable oil as the solvent.

Description

technical field [0001] The invention relates to a pesticide preparation, in particular to a microemulsion preparation using pine resin-based vegetable oil as a solvent and a preparation method thereof. Background technique [0002] For a long time, the production of domestic pesticide liquid preparations has widely used aromatic hydrocarbons (including benzene, toluene, xylene, etc.) organic solvents, polar solvents (such as methanol, N,N-dimethylformamide (DMF), cyclohexanone, etc.) etc., the annual consumption of "triphenyl" is as high as 200,000 to 300,000 tons, but these solvents have disadvantages such as low flash point, flammability and explosion, and high toxicity to humans and the environment. Organic solvents and additives will all enter the environment during the use of pesticides, polluting the environment and harming human health. [0003] In 1992, the U.S. government promulgated regulations prohibiting organic solvents such as toluene and xylene in pesticide p...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N25/04
Inventor 王文忠颜禧凯孔建颜禧童李谱超颜禧旋潘朝斌
Owner FUJIAN NUODE BIOTECH
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