Rear-earth surface-modified hollow glass microsphere and preparation method thereof
A hollow glass microsphere and surface modification technology, applied in chemical instruments and methods, inorganic pigment treatment, fibrous fillers, etc., can solve the problems of high cost, long process flow, unsuitable for large-scale industrialization, etc., and achieve low cost , the process is simple, the effect of improving the interface compatibility
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[0025] Example 1: 100 parts of hollow glass beads with an average particle diameter of 5 μm are stirred at 300 to 600 revolutions per minute in 300 parts of 0.1 mol / l sodium hydroxide solution at 80°C for 1 hour, and then filtered for use; 0.9g of lanthanum nitrate was fully dissolved in 299.1g of distilled water to prepare a 0.3% lanthanum nitrate solution; then the pretreated hollow glass beads were directly added to the rare earth solution, stirred to make it fully dispersed, The stirring time is controlled to be 15-20 minutes, and the stirring rate is controlled to 300-600 revolutions per minute. After the stirring is stopped, let it stand for 3 hours, then filter, wash with distilled water and dry for 2 hours at 100-120°C to obtain a modified product. Hollow glass beads.
Example Embodiment
[0026] Example 2: 100 parts of hollow glass beads with an average particle diameter of 10 μm are stirred at 300 to 600 revolutions per minute in 300 parts of 0.4 mol / l sodium hydroxide solution at 80°C for 1 hour, and then filtered for use; 3.6g of cerium nitrate was fully dissolved in 296.4g of distilled water to prepare a 1.2% cerium nitrate solution; then the pretreated hollow glass beads were directly added to the rare earth solution, stirred to make it fully dispersed, The stirring time is controlled to be 15-20 minutes, and the stirring rate is controlled to 300-600 revolutions per minute. After the stirring is stopped, let it stand for 3 hours, then filter, wash with distilled water and dry for 2 hours at 100-120°C to obtain a modified product. Hollow glass beads.
[0027] In order to test the modification effect, the hollow glass microbeads prepared without surface treatment and prepared by the surface treatment method of the present invention are blended with polypropyle...
Example Embodiment
[0028] Example 3: 100 parts of hollow glass beads with an average particle diameter of 30 μm are stirred at 300 to 600 revolutions per minute in 300 parts of 0.5 mol / l sodium hydroxide solution at 80°C for 1 hour, and then filtered for use; 6.0g of yttrium nitrate was fully dissolved in 294.0g of distilled water to prepare a 2.0% yttrium nitrate solution; then the pretreated hollow glass beads were directly added to the rare earth solution, stirred to make it fully dispersed, The stirring time is controlled to be 15-20 minutes, and the stirring rate is controlled to 300-600 revolutions per minute. After the stirring is stopped, let it stand for 3 hours, then filter, wash with distilled water and dry for 2 hours at 100-120°C to obtain a modified product. Hollow glass beads.
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