Method for preparing ceramic tile antifouling agent
An antifouling agent and ceramic tile technology, which can be applied to biocide-containing paints, antifouling/underwater coatings, coatings, etc., can solve the problems of complex preparation process, low composite antifouling efficiency, and poor long-term antifouling ability , to achieve excellent stain resistance, promote bonding, enhance gloss and texture
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Embodiment 1
[0026] The viscosity of 20 parts by mass at 25°C is 15mm 2 ·s -1 0.5 parts by mass of methyl hydrogen-containing silicone oil, the viscosity at 25°C is 300mm 2 ·s -1 0.5 parts by mass of methyl trifluoropropyl silicone oil and 0.5 parts by mass of aminopropyl aminosilicon oil with an ammonia value of 0.30±0.05 are added to 79 parts by mass of petroleum ether solvent at 25°C under stirring, and trifluoromethanesulfonic acid is added to adjust The pH value of the system is 6-7, and the mixing is continued for 10 minutes to obtain the ceramic tile antifouling agent of the present invention.
Embodiment 2
[0028] The viscosity of 5 parts by mass at 25°C is 45mm 2 ·s -1 10 parts by mass of methyl hydrogen-containing silicone oil, viscosity at 25°C is 100,000 mm 2 ·s -1 hydroxytrifluoropropyl silicone oil, 25 parts by mass of N-(β-aminoethyl) iminopropyl amino silicone oil with an ammonia value of 0.60±0.05, add 40 parts by mass of toluene, 20 parts by mass of toluene at 10°C under stirring In the mixed solvent of 1 part methyl ethyl ketone, trifluoromethanesulfonic acid is added to adjust the pH value of the system to 3-4, and the mixing is continued for 60 minutes to obtain the ceramic tile antifouling agent of the present invention.
Embodiment 3
[0030] The viscosity of 35 parts by mass at 25°C is 45mm 2 ·s -1 1 part by mass of methyl hydrogen-containing silicone oil, viscosity at 25°C is 10000 mm 2 ·s -1 Vinyl trifluoropropyl silicone oil, 4 parts by mass of N-(β-aminoethyl) iminopropyl amino silicone oil with an ammonia value of 0.85±0.05, add 60 parts by mass of cyclohexane at 10°C under stirring Add acetic acid and p-toluenesulfonic acid to the solvent to adjust the pH value of the system to 6-7, and continue mixing for 30 minutes to obtain the tile antifouling agent of the present invention.
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