Method for extracting peanut polysaccharides from hot pressed peanut meal
A technology for hot-pressed peanut meal and polysaccharide, which is applied in the directions of antitoxins, metabolic diseases, antitumor drugs, etc., can solve problems such as unsatisfactory extraction rate, avoid damage to the activity and safety of polysaccharides, mild reaction conditions, and improve extraction. The effect of efficiency
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Embodiment 1
[0020] The hot-pressed peanut meal is ultrafinely pulverized to 350 mesh, the raw material of the hot-pressed peanut meal is refluxed in 100ml of petroleum ether at 50°C for 8 hours, the petroleum ether is separated, and the hot-pressed peanut meal is dried to obtain dry powder of the hot-pressed peanut meal.
[0021] A citric acid-sodium citrate buffer solution system with a concentration of 0.1 mol / l is added to the dry powder of hot-pressed peanut meal, and the mass of the buffer solution added is 10 times the mass of the dry powder of hot-pressed peanut meal. Add cellulase, papain, acid protease to enzymatically hydrolyze peanut meal, the amount of added cellulase is 0.6% of the mass of hot-pressed peanut meal dry powder, the amount of papain is 0.05% of the mass of hot-pressed peanut meal dry powder, acid protease The dosage is 0.45% of the mass of hot-pressed peanut meal dry powder, and it is enzymatically hydrolyzed at 40°C and pH 5 for 2 hours.
[0022] After the enzym...
Embodiment 2
[0027] The hot-pressed peanut meal is ultrafinely pulverized to 400 mesh, the raw material of the hot-pressed peanut meal is refluxed in 100ml of petroleum ether at 50°C for 8 hours, the petroleum ether is separated, and the hot-pressed peanut meal is dried to obtain dry powder of the hot-pressed peanut meal.
[0028] Add a citric acid-sodium citrate buffer solution system with a concentration of 0.1mol / l to the hot-pressed peanut meal dry powder. The quality of the buffer solution added is 20 times the mass of the peanut meal dry powder. To decompose peanut meal, the added cellulase consumption is 0.6% of the dry powder quality of hot-pressed peanut meal, the consumption of papain is 0.15% of the dry powder quality of hot-pressed peanut meal, and the consumption of acidic protease is 0.6% of the dry powder quality of hot-pressed peanut meal. Enzymolysis was carried out at 50°C and pH7 for 250 minutes.
[0029] After the enzymatic hydrolysis, the reaction system was placed in ...
Embodiment 3
[0034] The hot-pressed peanut meal is ultrafinely pulverized to 500 mesh, the raw material of the hot-pressed peanut meal is refluxed in 100ml of petroleum ether at 50°C for 8 hours, the petroleum ether is separated, and the hot-pressed peanut meal is dried to obtain dry powder of the hot-pressed peanut meal.
[0035] A citric acid-sodium citrate buffer solution system with a concentration of 0.08 mol / l is added to the dry powder of peanut meal, and the mass of the buffer solution added is 20 times that of the dry powder of peanut meal. Add cellulase, papain, acid protease to enzymatically hydrolyze peanut meal, the amount of added cellulase is 0.7% of the mass of hot-pressed peanut meal dry powder, the amount of papain is 0.1% of the mass of hot-pressed peanut meal dry powder, acid The amount of protease is 0.6% of the mass of hot-pressed peanut meal dry powder. Enzymolysis was carried out at 50° C. and pH 5 for 3 hours.
[0036] After the enzymatic hydrolysis, the reaction ...
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