High-flame-retardant organic phosphate fire-proof plate capable of insulating heat and oxygen and suppressing smoke and preparation method thereof
A technology of flame retardant phosphate ester and fireproof board, applied in the field of building materials, can solve problems such as secondary pollution, and achieve the effect of flame retardant performance and environmental protection
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[0008] 1. Primary processing of raw materials: remove the weeds and moth-eaten and moldy parts in the wheat straw, cut them into small sections of 20cm-30cm, and use airflow drying method and drum dryer to dry;
[0009] 2. Binder preparation: Add 100kg of silica sol and 24.5kg of diethanolamine into a reaction kettle equipped with a stirring device, a reflux device and a temperature controller, heat to 60°C-90°C, react for 3h-5h, and then add acrylate Adjust the bonding strength for later use;
[0010] 3. Preparation of flame retardant: Add 100kg cyanuric chloride (I), 50kg ethanol, 158kg bishydroxyethylamine, 12kg sodium hydroxide and 62kg carbonic acid in a reaction kettle equipped with stirring device, reflux device and temperature controller Sodium, react at 70°C for 6h, cool the reaction mixture in the reactor to below 100°C, add 72kg of phosphorus pentoxide and 127kg of polyphosphoric acid, keep it at 100°C for 6h, and cool down to below 60°C to form High flame retardan...
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