Simplified preparation technology of rice oil
A technology for rice bran oil and rice bran, which is applied in the field of simplified rice bran oil preparation technology, can solve problems such as many optimization schemes, long refining time, easy spoilage, etc., achieves high chemical application value, improves refining yield, and slows down the effects of rancidity.
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Embodiment 1
[0017] Take 250g of rice bran that has been passed through a 40-mesh sieve and treated by microwave high heat for 4 minutes into the extraction kettle, start the extraction equipment, and send it to the CO 2 Add 5% wet-base ethanol as the entrainer to the fluid, set the extraction condition I to 15MPa, 30°C, and extract for 1.0h, and separate to obtain the bran oil I; increase the temperature and increase the pressure to condition II to 35MPa, 40°C, continue to extract for 4h, and separate to obtain Raw bran oil II, separation of defatted rice bran. The total extraction yield of bran oil was 14.83%; the yield of bran oil II was 14.35%, and the acid value was 14.98mgKOH / g.
[0018] Take the bran oil II in a centrifuge tube, quickly add diethanolamine with 8% oil weight, let it act in a constant temperature shaking box at 45°C (speed 100rpm) for 10 minutes, centrifuge (speed 3000rpm) for 30 minutes, separate the oil phase, and use oil weight 10% The oil phase was washed twice with ...
Embodiment 2
[0020] Take 250g of rice bran that has been passed through a 40-mesh sieve and treated by microwave high heat for 4 minutes into the extraction kettle, start the extraction equipment, and send it to the CO 2 Add 8% wet-base ethanol as the entrainer to the fluid, set the extraction condition I to 15MPa, 30°C, and extract for 1.0h, and separate to obtain the bran oil I; increase the pressure to condition II to 35MPa, 40°C, continue to extract for 4h, and separate Raw bran oil II, separation of defatted rice bran. The total extraction yield of bran oil was 15.12%; the yield of bran oil II was 14.69%, and the acid value was 13.95 mgKOH / g.
[0021] Take the bran oil II in a centrifuge tube, quickly add diethanolamine with 9% oil weight, let it act in a constant temperature shaking box at 50°C (speed 100rpm) for 15 minutes, centrifuge (speed 3000rpm) for 30 minutes, separate the oil phase, use 10% oil weight The oil phase was washed twice with deionized water and dried to obtain the fi...
Embodiment 3
[0023] Take 250g of rice bran that has been passed through a 40-mesh sieve and treated by microwave high heat for 6 minutes into the extraction kettle, start the extraction equipment, and send it to the CO 2 Add 8% ethanol as an entrainer to the fluid, set extraction condition I to 15MPa, 30°C, and extract 1.0h, and separate to obtain bran oil I; increase the pressure to condition II to 35MPa, 40°C, continue extraction for 4h, and separate to obtain bran oil II. Separate defatted rice bran. The total extraction yield of bran oil was 15.33%; the yield of bran oil II was 14.92%, and the acid value was 13.81 mgKOH / g.
[0024] Take the bran oil II in a centrifuge tube, quickly add diethanolamine with 11% oil weight, let it act in a constant temperature shaking box at 50°C (speed 100rpm) for 20 minutes, centrifuge (speed 3000rpm) for 30 minutes, separate the oil phase, use 10% oil weight The oil phase was washed twice with deionized water and dried to obtain the finished rice bran oil...
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