A multi-channel differential reaction device

A differential reaction, multi-channel technology, used in measurement devices, material separation, analysis of materials, etc., can solve problems such as insufficiency, eliminate gas composition and flow errors, ensure gas feeding, and reduce experimental deviations.

Active Publication Date: 2011-12-07
TIANJIN GOLDEN EAGLE TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, this document is only a micro-reactor device with a single pipeline, and only one catalyst can be evaluated at a time, which cannot satisfy the rapid evaluation and screening of multiple catalysts under the same reaction conditions.

Method used

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  • A multi-channel differential reaction device
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Experimental program
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Embodiment 1

[0028] The multi-channel differential reaction device of the present invention is used to carry out six groups of parallel ethanol etherification reactions simultaneously, and samples from the six channels are successively taken respectively for on-line analysis.

[0029] H on the device 2 , N 2 , exhaust gas and cooling water inlet and outlet, connect the corresponding channels respectively, connect the exhaust gas to the vent pipe and ensure that the vent pipe is unobstructed. When the system valve is closed, the six reaction tubes are filled with ZSM-5 catalyst, and the catalyst loading is 1.000g, and the reaction tubes are installed on the device in sequence. Turn on H 2Air source, guaranteed H 2 The pressure is maintained at 2.50MPa±0.1MPa, and the pressure difference between the two paths is controlled to be consistent. Adjust mass flow meter setting N 2 Gas velocity 200mL / min, H 2 The gas rate is 80mL / min. After the system pressure and gas flow are stable, turn on...

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Abstract

The invention discloses a multi-channel differential reaction device, and belongs to catalyst analysis and evaluation reaction device. The multi-channel differential reaction device comprises four systems of a gas-liquid charging system of (1)-(3), a multi-channel reactor system of (4)-(6), an automatic control system (7) and an on-line analysis system (8). The multi-channel differential reaction device adopts a high pressure distributor (4) to distribute a raw material into reaction tubes (6) of all channels. Temperatures of the all reaction tubes (6) are controlled unitedly by a heating furnace (5). The multi-channel differential reaction device is provided with the automatic control system (7) and the on-line analysis system (8) and can satisfy that in a reaction process, at any time, reaction products in all channel reaction tubes can be taken out on line simultaneously, are placed respectively in corresponding quantitative rings and are analyzed orderly through use of a gas chromatography. The catalyst analysis and evaluation reaction device can evaluate a catalyst rapidly and also evaluate and screen multiple catalysts simultaneously under a condition thus saves time spent on research and exploitation of a novel catalyst.

Description

Technical field: [0001] The invention is a multi-channel differential reactor device, which belongs to the category of catalyst analysis and evaluation reaction devices, and is used in the screening and evaluation research of general gas-solid phase reaction catalysts, such as the catalytic conversion of biomass oil into high-quality fuel Oil energy chemical technology research. Background technique: [0002] With the rapid development of the domestic petroleum and chemical industry, more and more companies and enterprises regard technological improvement and technological innovation as the focus of scientific research, so the rapid and accurate development of high-efficiency catalysts has become a key technology in this industry. In the development and research of bio-oil high-quality energy and chemical processes such as bio-oil catalytic cracking, catalytic hydrogenation, and catalytic pyrolysis hydrogen production, micro-reactor equipment is inseparable. [0003] Howeve...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/00B01J8/06G01N30/02G01N30/06
Inventor 乔冠东
Owner TIANJIN GOLDEN EAGLE TECH
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