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248results about How to "Control dwell time" patented technology

Method for treating desulfurization ash

The invention discloses a method for treating desulfurization ash. The method comprises the following steps of: mixing the desulfurization ash generated by a dry/semidry desulphurization process and limestone powder, which serve as raw materials of a desulfurizer in a wet flue gas desulfurization process, according to a proportion; uniformly stirring the desulfurizer and pumping the desulfurizer into a slurry pond of an absorption tower; adding a catalyst into the slurry pond; introducing oxidation air into the slurry pond; introducing flue gas into the slurry pond through a flue; reacting the desulfurizer with SO2 in the flue gas under the action of the oxidation air and the catalyst; controlling the pH value of the slurry in the absorption tower, the slurry temperature, the content of solid matters contained in the slurry and the retention time of the desulfurizer in the slurry pond; after the reaction is completed, performing vortex concentration and vacuum filtration to obtain a gypsum by-product; and adding wastewater produced in the process into a process water collection box for recycling. The method is simple, is easy to realize, has remarkable effect, provides a safe and proper treatment way for the dry/semidry desulfurization ash and has good economic and social benefits.
Owner:BAOSHAN IRON & STEEL CO LTD

Spiral push type low temperature pyrolysis carbonation furnace

The invention discloses a spiral push type low temperature pyrolysis carbonation furnace which comprises a bracket and a furnace body, wherein the furnace body is provided with a feed port and a discharge hole; the furnace body comprises an inner heating cylinder and an outer heating cylinder which are sleeved together; the tail end of the inner heating cylinder penetrates out of the outer heating cylinder; the tail end of the inner heating cylinder is provided with an tail gas outlet; the outer heating cylinder is provided with a high temperature smoke gas inlet and a high temperature smoke gas outlet; a plurality of deflectors are misplaced on the inner wall of the outer heating cylinder and the outer wall of the inner heating cylinder; and a plurality of hollow material transportation screws penetrate through the furnace, and the inside of the furnace body is provided with an electricity or smoke gas heating device. Because a double-layer tube-in-tube structure and a spiral push type pyrolysis carbonation mode are adopted and the tail gas outlet is arranged at the tail end of the inner heating cylinder, the spiral push type low temperature pyrolysis carbonation furnace has the characteristics that raw material adaptability is wide and a structure is simple, tail gas waste heat and low-grade pyrolysis carbonized gas can be fully utilized, thermal efficiency is high, and the like.
Owner:江苏华威龙玖环保科技有限公司

Biomass spiral pyrolysis device and pyrolysis process

The invention relates to a biomass pyrolysis device and a process thereof. The device comprises a charging system, a spiral pyrolysis reactor and a product collection system, wherein a rotating shaft which is communicated with a variable-frequency motor and provided with a spiral propeller is arranged in center holes on two end covers of a cylinder body of the reactor; the side wall of the cylinder body is provided with a biomass feed pipe and a pyrolysis product outlet pipe; the outlet pipe is vertically extended into a coke collection tank; and the coke collection tank are communicated with a condenser, a bio-oil collection tank and a tail gas discharge pipe in turn through an air outlet pipe on the side wall. The process comprises the following technological processes: firstly, starting an external heating system to ensure that the temperature in a reactor is between 500 and 550 DEG C; secondly, putting biomass granular raw materials into the reactor through an inlet pipe, simultaneously starting the variable-frequency motor, and determining the rotating speed n of the variable-frequency motor according to the set residence time t, and the axial length L and the screw pitch l of the spiral propeller; and finally, starting the pyrolysis product collection system. The biomass pyrolysis device can accurately control the pyrolysis time and control the pyrolysis temperature in a partitioning mode so that the obtained bio-oil components are controllable and are easy to extract chemical products.
Owner:UNIV OF SCI & TECH OF CHINA

Separation method of olefin hydroformylation reaction liquid-phase discharged material

The invention relates to a separation method of an olefin hydroformylation reaction liquid-phase discharged material. The invention belongs to the field of hydroformylation reaction aldehyde preparation. The method comprises the steps that: (1) decompression is carried out upon a C2-C4 olefin hydroformylation liquid-phase discharged material; (2) the decompressed C2-C4 olefin hydroformylation liquid-phase discharged material is subjected to multi-level heating evaporation separation, wherein the pressure after decompression is corresponding to the evaporation temperature, and the evaporation temperature is no higher than 140 DEG C; (3) gas-phase materials obtained in each level of evaporation separation are condensed, such that a liquid-phase aldehyde product is obtained; and (4) a catalyst-containing liquid-phase material obtained through the multi-level evaporation separation is recycled to the reactor. With the technical scheme provided by the invention, the separation of the hydroformylation reaction product and a catalyst solution can be carried out under a relatively low temperature. With leveled evaporation, the retention time of the materials in a hot area in the separation process can be effectively controlled, such that the heat-sensitive rhodium catalyst can be protected.
Owner:CHINA PETROLEUM & CHEM CORP +1

Microchannel plate with fractal structure, photocatalytic reactor and application thereof

The invention provides a microchannel plate with a fractal structure, a photocatalytic reactor and an application thereof. The microchannel plate with the fractal structure comprises a first surface and a second surface which are opposite; the first surface and the second surface of the microchannel plate with the fractal structure each is provided with a main pipeline microchannel and multistage H-shaped fractal bifurcated microchannels which are connected with one end of the corresponding main pipeline microchannel, and the H-shaped fractal bifurcated microchannels of the first surface of the microchannel plate with the fractal structure communicate with those of the second surface of the microchannel plate with the fractal structure through connecting through holes. According to the microchannel plate with the fractal structure, the photocatalytic reactor and the application thereof, through forming fractal-structured microchannels in the upper and lower surfaces of the microchannel plate with the fractal structure, three phases, i.e., gas, liquid and solid phases can be effectively distributed, heat transfer and mass transfer are strengthened, the problem in collection of reactants of fractal distribution can be effectively solved, meanwhile, the length of the microchannels can be increased, and the control on reaction flux and reactant residence time is better facilitated.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI

High-throughput preparation device and method for high-silicon aluminum alloy structural gradient material used for packaging

The invention discloses a high-throughput preparation device and method for a high-silicon aluminum alloy structural gradient material used for packaging. The device comprises an upper high-temperature die, outer die moulds, induction coils, a gradient workpiece, cooling water circulating devices, a lower low-temperature die and thermocouples, wherein the upper high-temperature die is used for keeping the inner temperature of the whole die balancing and supplying a certain heat source to atomized powder of the high-silicon aluminum alloy; the outer die moulds are used for positioning two or three kinds of the prepared atomized powder of the gradient high-silicon aluminum alloy; the atomized powder of the high-silicon aluminum alloy is fed based on the sequence that the low-component alloy powder is at the bottom end of each outer die mould, and the high-component aluminum powder is at the top end of each outer die mould; the induction coils can be used as movable induction heating elements for supplying heat to the whole preparation process; the gradient workpiece is used for preparing the gradient material; the cooling water circulating devices can be used for exporting excess heat when the temperature in the preparation process is beyond a set temperature; the temperature of the lower low-temperature die is in contrast to the temperature of the upper high-temperature die, so that temperature gradient can be generated; the thermocouples are used for testing the temperature and controlling the induction heating time, so as to generate the temperature gradient. The alloy prepared by the device and the method is high in density, and the structure is refined, so that the alloy is outstanding in comprehensive performances.
Owner:SUZHOU XINHUILIAN SEMICON TECH CO LTD

Method for preparing cyclopropyl methyl ketone

The invention relates to a method for preparing cyclopropyl methyl ketone, and belongs to the field of organic synthesis. The preparing method includes the following steps that metal halide and an inert solvent are added into a fixed bed reactor, the fixed bed reactor is heated to 185-195 DEG C, and then alpha-acetyl-gamma-butyrolactone is continuously added into the fixed bed reactor, and is subjected to a cleavage reaction; after the reaction is saturated, the alpha-acetyl-gamma-butyrolactone stops to be added, reaction distillation continues to be carried out till no product is distilled out, and a cyclopropyl-methyl-ketone crude product is obtained; the fixed bed reactor is connected with a rectifying tower, the prepared cyclopropyl-methyl-ketone crude product is transferred into the rectifying tower to be subjected to high tower dividing and then subjected to normal pressure rectification, the reflux ratio is adjusted, impurities are separated, and the high-purity cyclopropyl methyl ketone is obtained through distilling. The method is low in production cost, high in production efficiency, product yield and purity, small in by-product number, wastewater amount, waste material number and environment pollution and more suitable for industrial production.
Owner:LINHAI LIANSHENG CHEM

Pyrolysis method and device of low speed bed

The invention provides a low velocity bed pyrolysis method and a device; fuel is added from a pyrolysis chamber so as to generate pyrolysis gas and semi-coke; the semi-coke is sent to a combustion chamber so as to be burned; the generated high-temperature material enters the pyrolysis chamber again from top of a material returning device, thus providing heat for the pyrolysis reaction; the combustion chamber is a circular fluidized bed type and the oxygen content of smoke at an outlet is zero; the semi-coke and low-temperature material are exhausted from the pyrolysis chamber and enter the combustion chamber through a pneumatic control valve; the pyrolysis chamber is internally provided with the low velocity bed; the fluidized air quantity of material returning device and the pneumatic control valve is adjusted so as to adjust the material height inside the pyrolysis chamber and the staying time of the material inside the pyrolysis chamber; the quantity of the air which enters the combustion chamber is adjusted so as to adjust the combustion heat exhausting quantity of the fuel, thus adjusting the temperature of the pyrolysis chamber; the pyrolysis chamber runs in a way of the combination of a low speed fluidized bed and a movable bed; the material has long staying time inside the pyrolysis chamber and complete pyrolysis reaction; the method and the device have various control ways of well controlling the temperature of the pyrolysis chamber. The method and the device can be used for coal, biomass and other carbonaceous refuse and alternative fuels, thus generating pyrolysis gas and coal tar.
Owner:INST OF ENGINEERING THERMOPHYSICS - CHINESE ACAD OF SCI

Catalyst distillation column internals for high effective mass transfer

The invention relates to an internal part of a high efficient mass transfer catalytic distillation tower. Wherein, the internal part 1 is composed of a porous container and a filler 5 with catalytic performance therein, the side wall and the lower bottom surface of the container are fixed, at least one longitudinal sliding bar 7 is arranged at the middle part of the lower bottom surface, the upper bottom surface can move up and down along the longitudinal sliding bar and be fixed at an arbitrary height of the sliding bar by a bolt 8, the side wall 2 of the container is not transparent, the upper bottom surface 4 and the lower bottom surface 3 of the container are wire screen plates or porous plates, the internal part is fixed on a grid-shaped support 10 by a nut 9, and the grid-shaped support is fixed on the wall 13 of the catalytic distillation tower. The height of the upper bottom surface of the internal part of the catalytic distillation tower of the invention is lower than the side wall, thereby accumulating liquid with a certain height above a catalyst; reactants are promoted to enter a catalyst bed with the help of the gravity of the liquid, thereby allowing the reactants to be fully contacted with the surface of the catalyst; products are simultaneously impelled to be moved out of the catalyst bed, thereby avoiding the excessive reaction and effectively controlling the retention time of the reactants on the surface of the catalyst.
Owner:TIANJIN UNIV

Power tube driving system and method

ActiveCN106954123AControl dwell timeSuppression of radiated electromagnetic interferenceSignal processingTransducer circuitsCharge currentParasitic capacitance
The invention provides a power tube driving system and method. The system comprises a driving circuit part of the lower tube of a power tube and a driving circuit part of the upper tube of the power tube. The driving circuit part of the lower tube of the power tube is configured to control the residence time of the lower tube of the power tube on a Miller platform by controlling the size of the first charging current for charging the stray capacitance of the lower tube of the power tube through a first switching circuit, and / or, control the residence time of the lower tube of the power tube on the Miller platform by controlling the size of the first discharging current for discharging the stray capacitance of the lower tube of the power tube through a second switching circuit. The driving circuit part of the upper tube of the power tube is configured to control the residence time of the upper tube of the power tube on the Miller platform by controlling the size of second discharging current for discharging the stray capacitance of the upper tube of the power tube through a third switching circuit, and / or, control the residence time of the upper tube of the power tube on the Miller platform by controlling the size of second charging current for charging the stray capacitance of the upper tube of the power tube through a fourth switching circuit.
Owner:ON BRIGHT ELECTRONICS SHANGHAI

Method for synthesizing 3-fluoro-4-(4-morpholinyl)aniline by using micro-channel reactor

ActiveCN106397358AReduce energy consumptionEfficient mass and heat transferOrganic chemistryAcetic acidHydrogen
The invention provides a method for synthesizing 3-fluoro-4-(4-morpholinyl)aniline by using a micro-channel reactor. The micro-channel reactor comprises a preheating module group composed of one or more parallely-connected preheating modules and a reaction module group composed of one or more tandemly-connected reaction modules, wherein the preheating module group is series connection with the reaction module group. The method comprises the following steps: separately preheating difluorobenzene, concentrated nitric acid and concentrated sulfuric acid, then subjecting the preheated difluorobenzene, concentrated nitric acid and concentrated sulfuric acid to a reaction in the reaction module group and carrying out treatment so as to obtain 3,4-difluoronitrobenzene; dissolving 3,4-difluoronitrobenzene in an organic solvent, adding organic base, dissolving morpholine in the organic solvent, carrying out preheating, allowing the obtained solution to enter the reaction module group for a reaction and carrying out treatment so as to obtain 4-(2-fluoro-4-nitrophenyl)morpholine; and dissolving 4-(2-fluoro-4-nitrophenyl)morpholine in ethyl acetate, adding a catalyst, carrying out preheating, allowing the obtained solution and hydrogen to enter the reaction module group for a reaction and carrying out treatment so as to obtain 3-fluoro-4-(4-morpholinyl)aniline. The method has the advantages of low energy consumption, high yield, high product purity, safety, flexibility, etc.
Owner:HEILONGJIANG XINCHUANG BIOLOGICAL TECH DEV CO LTD

Ion source with ultra-large ion beam divergence angle

InactiveCN102779711ARealize spatial scanningRealize spatial divergence angle controlElectric discharge tubesDivergence angleIon beam-assisted deposition
The invention relates to an ion source used in an optical vacuum coating machine (ion beam auxiliary deposition equipment) or ion beam sputtering and etching equipment, in particular to the ion source with an ultra-large ion beam divergence angle. The technical scheme is that the ion source comprises a gas discharge chamber, wherein an insulating end cover is arranged at one end of the gas discharge chamber; and a focusing magnetic field generating unit and a magnetic field scanning unit are arranged outside the insulating end cover. Through a group of orthogonal magnetic field, the direction of an ion beam led into the magnetic field is controlled, and by setting the voltage change rule of electromagnetic coils in an X direction and a Y direction, space scanning on the ion beam can be realized. Controlling over the space divergence angle of the ion beam can be realized by adjusting the current magnitude of the electromagnetic coils. Compared with the prior art, the ion source has the advantages that 1, the divergence angle of the ion beam output by the ion source can be up to 180 degrees; 2, the divergence angle of the ion beam can be adjusted according to practical needs, and the requirement of different thin film deposition processes can be met; and 3, the uniformity of the flow density of the ion beam is high.
Owner:XIAN TECHNOLOGICAL UNIV

Spiral filtration dehydrator

The invention is widely applicable to the technical field of dehydration of paper mill sludge, electroplating sludge, leather sludge, domestic sludge and various types of sludge and particularly relates to a spiral filtration dehydrator. The spiral filtration dehydrator comprises a rack, wherein two spiral shafts are arranged on the rack in parallel, one end of each spiral shaft is connected with a spindle driving device, the two spiral shafts are respectively installed in two filter cartridges, towing wheel shafts are arranged between the outer side walls of the two filter cartridges and the two filter cartridges, one end of each towing wheel shaft is connected with a driving device, two ends of each filter cartridge are respectively a feeding port and a discharging port, the rack is provided with blanking port corresponding to the discharging ports, filtrate outlets are respectively formed in the middle positions, corresponding to the filter cartridges, on the rack, bristle brush roller devices are respectively arranged above the two filter cartridges, and a flushing water device is arranged on one side of the bristle brush roller devices. The spiral filtration dehydrator can decrease flocculant usage amount, adjust spiral and the roller rotation speed according to feeding concentration and control the staying and dehydration time of the sludge in a device. A dehydration effect is good, and material requirements are low. The outlet sludge concentration is adjustable, automatic operation is achieved, and labor intensity is low.
Owner:SHANDONG CHENZHONG MACHINERY
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