A method for preparing high-purity low-sulfur expanded graphite
A technology of expanded graphite and high-purity graphite, applied in the electrolysis process, electrolysis components and other directions, can solve the problems of high production cost and low product purity, and achieve the effects of low production cost, simple method and low pollution
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specific Embodiment approach 1
[0012] Specific embodiment one: the method for preparing high-purity low-sulfur expanded graphite in this embodiment is carried out according to the following steps:
[0013] 1. Put the phosphorus flake graphite in the graphitization furnace, heat it to 2800°C, keep it warm for 2 hours, then introduce chlorine gas, and continue heating until the carbon content is ≥ 99.9% (mass), to obtain the phosphorus flake high-purity graphite;
[0014] 2. Put the phosphorus flake high-purity graphite obtained in step 1 into a polypropylene mesh bag, then soak in peroxide water for 24 hours, and then lift it up to drench;
[0015] 3. After soaking in peroxide water, the polypropylene mesh bag containing phosphorus sheet high-purity graphite is used to wrap the graphite block as an anode, put it into the graphite electrolytic cell, and then inject the electrolyte, which is composed of ammonium salt solution and acid Prepared, with graphite as the cathode, and then at a current density of 0.1...
specific Embodiment approach 2
[0019] Embodiment 2: The difference between this embodiment and Embodiment 1 is that in step 3, the mass ratio of the phosphorus flake high-purity graphite to the ammonium salt is 1:1.5-4.5. Other steps and parameters are the same as in the first embodiment.
specific Embodiment approach 3
[0020] Specific embodiment three: the difference between this embodiment and specific embodiment one is: in step three, the mass ratio of the phosphorus flake high-purity graphite to the ammonium salt is 1:2-4. Other steps and parameters are the same as in the first embodiment.
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