Amur corktree bark extract-containing natural antibacterial textile and preparation method thereof
A Phellodendron phellodendron extract, a natural antibacterial technology, applied in the field of textiles, can solve the problems that have not been solved, and achieve the effect of strong antibacterial activity, simple preparation process, and obvious antibacterial effect
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Embodiment 1
[0019] Embodiment 1 A kind of preparation method of the natural antibacterial textile containing Phellodendron Phellodendron extract
[0020] (1) Preparation of microcapsules: Weigh 10 parts of Phellodendron Phellodendri extract, 1 part of polyvinyl alcohol, 30 parts of glutaraldehyde, and 2 parts of emulsifier, mix Phellodendron Phellodendri extract and polyvinyl alcohol aqueous solution, mix well and inject 1 part of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed, and the rotation speed is 700r / min to prepare emulsion A; mix glutaraldehyde with 5 drops of 10% hydrochloric acid aqueous solution, mix well and inject another part of the continuous phase n-hexane containing 1 part of emulsifier High-speed emulsification in alkanes, rotating speed 700, to prepare emulsion B; mix the two emulsions A and B at 10°C, and stir at high speed for 0.5h, filter, wash with petroleum ether for 3 times, and freeze-dry at -10°C to obtain microcapsules;
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Embodiment 2
[0029] Embodiment 2 A kind of preparation method of the natural antibacterial textile containing Cortex Phellodendri extract
[0030] (1) Preparation of microcapsules: Weigh 30 parts of Phellodendron Phellodendri extract, 10 parts of polyvinyl alcohol, 60 parts of glutaraldehyde, and 30 parts of emulsifier, mix the Phellodendron Phellodendri extract and polyvinyl alcohol aqueous solution, mix well and inject 15 parts of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed and the rotation speed is 2500r / min to prepare emulsion A; mix glutaraldehyde with 10 drops of 30% hydrochloric acid aqueous solution, mix well and inject another part of the continuous phase n-hexane containing 15 parts of emulsifier Emulsion B was prepared by high-speed emulsification in alkanes at a speed of 2500r / min; the two emulsions A and B were mixed at 30°C, stirred at high speed for 2 hours, filtered, washed 5 times with petroleum ether, and freeze-dried at -5°C to obtain ...
Embodiment 3
[0039] Embodiment 3 A kind of preparation method of the natural antibacterial textile containing Cortex Phellodendri extract
[0040] (1) Preparation of microcapsules: Weigh 20 parts of Phellodendron Phellodendri extract, 5 parts of polyvinyl alcohol, 40 parts of glutaraldehyde, and 20 parts of emulsifier, mix the Phellodendron Phellodendri extract and polyvinyl alcohol aqueous solution, and inject 10 parts of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed and the rotation speed is 2000r / min to prepare emulsion A; mix glutaraldehyde with 7 drops of 20% hydrochloric acid aqueous solution, mix well and inject another continuous phase n-hexane containing 10 parts of emulsifier Emulsion B was prepared by high-speed emulsification in alkanes at a speed of 2000r / min; the two emulsions A and B were mixed at 20°C, stirred at high speed for 1 hour, filtered, washed 4 times with petroleum ether, and freeze-dried at -8°C to obtain microcapsules;
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