Preparation method and application method of anti-fake microspheres
A technology of microspheres and colors, applied in non-fiber pulp addition, papermaking, textiles and papermaking, etc., can solve the problems of high cost, complex synthesis process and equipment of anti-counterfeiting resin microspheres and fluorescent anti-counterfeiting point materials, and low yield, etc. To achieve the effect of improving the difficulty of imitation
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Embodiment 1
[0024] The first step, the configuration of raw materials
[0025] Weigh 0.5 grams of long-wave fluorescent blue anti-counterfeiting material, 0.5 grams of benzoyl peroxide, 82.5 grams of methyl acrylate and 17.5 grams of divinylbenzene;
[0026] The second step, the dissolution of raw materials
[0027] Dissolve the long-wave fluorescent blue anti-counterfeiting material and benzoyl peroxide weighed in the first step in the methyl acrylate and divinylbenzene weighed in the first step, and then pour the resulting mixed solution into 400 ml In the there-necked bottle of 1000 milliliters of the aqueous solution of polyvinyl alcohol and sodium dodecylbenzenesulfonate, wherein the mass percent concentration of polyvinyl alcohol and sodium dodecylbenzenesulfonate in the aqueous solution is the same as 1%;
[0028] The third step, synthesis reaction
[0029] Stir the liquid obtained in the second step, while heating to 45°C, then raise the temperature to 80°C in 1 hour, and keep t...
Embodiment 2
[0034] The first step, the configuration of raw materials
[0035] Weigh 0.85 grams of warm red anti-counterfeiting material, 0.5 grams of benzoyl peroxide, 82.5 grams of methyl acrylate and 17.5 grams of divinylbenzene;
[0036] The second step, the dissolution of raw materials
[0037] Dissolve the temperature-changing red anti-counterfeiting material and benzoyl peroxide weighed in the first step in the methyl acrylate and divinylbenzene weighed in the first step, and then pour the resulting mixed solution into 400 ml In the there-necked bottle of 1000 milliliters of the aqueous solution of polyvinyl alcohol and sodium dodecylbenzenesulfonate, wherein the mass percent concentration of polyvinyl alcohol and sodium dodecylbenzenesulfonate in the aqueous solution is the same as 1%;
[0038] The third step, synthesis reaction
[0039] Stir the liquid obtained in the second step, heat up to 45°C at the same time, then raise the temperature to 80°C in 1 hour, and keep the tempera...
Embodiment 3
[0044] The first step, the configuration of raw materials
[0045] Weigh 0.35 grams of infrared green anti-counterfeiting material, 0.5 grams of benzoyl peroxide, 82.5 grams of methyl acrylate and 17.5 grams of divinylbenzene;
[0046] The second step, the dissolution of raw materials
[0047] Dissolve the infrared green anti-counterfeiting material and benzoyl peroxide weighed in the first step in methyl acrylate and divinyl benzene weighed in the first step, and then pour the resulting mixed solution into 400 ml of In the there-necked bottle of 1000 milliliters of the aqueous solution of polyvinyl alcohol and sodium dodecylbenzene sulfonate, wherein the mass percentage concentration of polyvinyl alcohol and sodium dodecylbenzene sulfonate in aqueous solution is the same as 1%;
[0048] The third step, synthesis reaction
[0049] Stir the liquid obtained in the second step, heat up to 45°C at the same time, then raise the temperature to 80°C in 1 hour, and keep the temperat...
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