Identification and detection method for nanometer titanium dioxide in paints

A nano-titanium dioxide and detection method technology, which is applied in the field of chemical substance detection, can solve the problems of large surface tension of nano-material particles, lack of detection standards for nano-coatings, and difficult application, and achieve simple and effective pre-treatment processes

Inactive Publication Date: 2012-04-18
CHINESE ACAD OF INSPECTION & QUARANTINE
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] 1. The surface tension of nanomaterial particles is very large and easy to agglomerate;
[0008] 2. Nanomaterials are high-tech products, and how to characterize their application in coatings is a difficult problem;
[0009] 3. Nano materials have special properties different from other traditional materials, so the construction and storage methods of traditional coatings are not suitable for nano coatings;
[0010] 4. Nano-coatings lack relevant testing standards, such as the purity, particle size, particle size distribution, storage stability and other indicators and testing method standards of nano-pigments in coatings have not been perfected
[0011] It can be seen that the evaluation system of nano-coatings is still blank, because the lack of a standard evaluation system for nano-materials greatly limits the application of nano-coatings.
The current evaluation system only evaluates from the performance of coatings and coating films, and has not established an in-depth evaluation system, which seriously hinders the development of nano coatings.

Method used

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  • Identification and detection method for nanometer titanium dioxide in paints
  • Identification and detection method for nanometer titanium dioxide in paints
  • Identification and detection method for nanometer titanium dioxide in paints

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Embodiment Construction

[0040] For further illustrating the present invention, specifically illustrate in conjunction with following examples:

[0041] 1. Chemical reagents and instruments used in the examples

[0042] Ethanol was purchased from Beijing Chemical Plant, and the specification was analytically pure; deionized water was obtained from the Mili-Q ultrapure water preparation instrument in the United States. The specific instrument information is shown in Table 1.

[0043] Table 1 Experimental instruments and their manufacturers, instrument models

[0044]

[0045] 2, the experimental process of embodiment

[0046] Except for the quantitative experiment, the samples in other experiments were in powder form. Apply the coating evenly on a smooth glass plate, put it in an oven, heat it at 80°C for 12 hours, after the coating film is completely dry, scrape off the coating film and put it in an agate mortar for grinding until the sample is ground into powder .

[0047] 3, the experimental...

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Abstract

The invention provides an identification and detection method for nanometer titanium dioxide in paints. According to the invention, qualitative and quantitative analysis of nanometer titanium dioxide in the paints is successfully carried out, and the technology of identification and detection of nanometer titanium dioxide in the paints is successfully realized through identification of the crystal structure and crystal microstructure characteristics of a nano-material and crystal morphology, particle size, distribution and the like of the nano-material by using powder X ray diffraction analysis (XRD), scanning electron microscope analysis (SEM) and spectral analysis. Meanwhile, the method of integrating sphere reflection is utilized to determine ultraviolet ray absorption of nanometer titanium dioxide in four paints, which provides reasonable evidence to the fact that nanometer titanium dioxide can be used as an additive for ultraviolet ray resisting or antibiosis paints.

Description

technical field [0001] The invention relates to the technical field of chemical substance detection, in particular to a detection method of nanometer titanium dioxide in paint. Background technique [0002] Due to the small size effect, surface effect, quantum size effect and macroscopic quantum tunneling effect, nanoparticles are different from conventional particles in terms of heat, magnetism, light, sensitivity and surface stability. Use the anti-ultraviolet, photocatalysis, anti-mildew, anti-bacterial, conductive and other properties of nanoparticles to modify traditional coatings, so that the coatings have some special functions such as: anti-aging, anti-bacterial, anti-fouling, conductive, stealth, etc. [0003] Nano-coatings are generally composed of nano-materials and organic coatings. Therefore, more scientifically, they should be called nanocomposite coatings. Only when two conditions are met can it be called a nano-coating: one is that the coating contains at le...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/44G01N23/20G01N21/65G01N21/71G01N15/02G01N23/22
Inventor 杨海峰卢晓静闫妍李俊芳
Owner CHINESE ACAD OF INSPECTION & QUARANTINE
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