Contrast Chinese patent medicine extract of pills of six ingredients with rehmannia, and preparation method and application thereof
A technology for Liuwei Dihuang Pills and Chinese patent medicines, which is applied in the field of Chinese medicine component analysis, can solve the problems of complex operation, unfavorable inspection, long inspection period, etc., achieves high separation degree and stability, improves quality control level, and reduces inspection costs.
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Embodiment 1
[0032] Example 1 Liuwei Dihuang Pills Control Chinese Patent Medicine Extract
[0033] (1) Preparation of Liuwei Dihuang pill control Chinese patent medicine extract
[0034] 1) Preparation of Liuwei Dihuang Pills as a control Chinese patent medicine: take 160 g rehmannia glutinosa, 80 g wine cornus, 60 g moutan cortex, 80 g yam, 60 g Poria cocos and 60 g Alisma, grind them into fine powder, pass through a 40-mesh sieve, Mix well; add 100g of refined honey to every 100g of powder to make Liuwei Dihuang Pills as a Chinese patent medicine;
[0035] 2) Preparation of Liuwei Dihuang Pills control Chinese patent medicine extract: Take 15g of Liuwei Dihuang Pills as a control Chinese patent medicine, put it into a stoppered Erlenmeyer flask, add 200mL of methanol, ultrasonically extract for 25 minutes, filter, and add the filtrate to a neutral alumina column (100-200 mesh, 10g, inner diameter 1cm), elute with 100mL methanol, collect the eluate, evaporate to 50mL, transfer to a 10...
Embodiment 2
[0055] Example 2 Detection of Commodity Contents of Commercialized Liuwei Dihuang Pills
[0056] 1) The Liuwei Dihuang Pill prepared in Example 1 was used as the standard substance for the detection of the control Chinese patent medicine extract;
[0057] 2) Processing of commercial Liuwei Dihuang Wan samples: Weigh 1 g of 26 batches of commercial Liuwei Dihuang Wan from different manufacturers in the market, put them in a stoppered Erlenmeyer flask, add 30 mL of methanol, extract by ultrasonic for 25 minutes, filter, and evaporate the filtrate to to 5mL, transfer to a 10mL volumetric flask, add methanol to the mark, and prepare the test solution;
[0058] 3) Detection: High performance liquid chromatography is used for detection, and the detection conditions are as follows:
[0059] Chromatographic column: octadecyl bonded silica gel as filler;
[0060] Mobile phase: mobile phase A is acetonitrile, mobile phase B is 0.05% phosphoric acid water;
[0061] Gradient elution:...
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