Preparation method of epoxy resin grafted montmorillonite filler
A technology of epoxy resin and montmorillonite, which is used in fibrous fillers, anti-corrosion coatings, dyed polymer organic compounds, etc., can solve problems such as poor interface compatibility, improve corrosion resistance and service life, and eliminate defects and porosity effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0026] Add 100 grams of montmorillonite with a cation exchange capacity of 90 meq / 100 g into 4 liters of deionized water, and vigorously stir at 80° C. for 4 hours to obtain a stable montmorillonite suspension. Take 33 grams of tetraethylenepentamine and add it to 600 milliliters of deionized water, drop in hydrochloric acid equivalent to tetraethylenepentamine and stir for 30 minutes to prepare a quaternary ammonium salt. At this time, an amino group on the quaternary ammonium salt molecule has undergone quaternary reaction, while the remaining amino groups remain. Drop the quaternary ammonium salt solution into the montmorillonite suspension heated to 80°C, stir vigorously at 80°C for 2 hours, cool to room temperature, filter, and then wash repeatedly with deionized water until no chlorine can be detected with silver nitrate solution ion so far. The samples were dried at room temperature for 72 hours, and then dried in a vacuum oven at 60°C for 48 hours to remove residual m...
Embodiment 2
[0029] Add 100 grams of montmorillonite with a cation exchange capacity of 100 meq / 100 g into 3.5 liters of ethanol, and vigorously stir at 80° C. for 2 hours to obtain a stable montmorillonite suspension. Get 35 grams of diaminodiphenylmethane and add it to 500 milliliters of deionized water, drop in sulfuric acid equivalent to diaminodiphenylmethane and stir at 80°C for 30 minutes to prepare a quaternary ammonium salt. At this time, one of the quaternary ammonium salt molecules The amino group has been quaternized while the other amino group remains. Drop the quaternary ammonium salt solution into the montmorillonite suspension heated to 80°C, stir vigorously at 80°C for 2 hours, cool to room temperature, filter, and then wash repeatedly with deionized water until no chlorine can be detected with silver nitrate solution ion so far. The samples were dried at room temperature for 72 hours, and then dried in a vacuum oven at 60°C for 48 hours to remove residual moisture. The ...
Embodiment 3
[0032] Add 100 grams of montmorillonite with a cation exchange capacity of 85 meq / 100 g into 1 liter of isopropanol, and vigorously stir at 80° C. for 2 hours to obtain a stable montmorillonite suspension. Take 28 grams of 6-aminocaproic acid and add it to 600 milliliters of deionized water, drop in benzenesulfonic acid equivalent to 6-aminocaproic acid and stir at 80°C for 30 minutes to prepare a quaternary ammonium salt. The amino group has been quaternized while the other carboxyl group remains. Drop the quaternary ammonium salt solution into the montmorillonite suspension heated to 80°C, stir vigorously at 80°C for 2 hours, cool to room temperature, filter, and then wash repeatedly with deionized water until no chlorine can be detected with silver nitrate solution ion so far. The samples were dried at room temperature for 72 hours, and then dried in a vacuum oven at 60°C for 48 hours to remove residual moisture. The dried sample was ground and passed through a 300-mesh s...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com