Hydrophilic ultraviolet light curing coating and preparation method thereof
A technology of curing coatings and ultraviolet light, applied in epoxy resin coatings, polyurea/polyurethane coatings, coatings, etc., can solve the problems of increased energy consumption, the hydrophilicity does not meet practical requirements, and the hydrophilic angle is small.
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[0077] The preparation method of waterborne epoxy acrylic resin is as follows:
[0078] Add 3 mol of epoxy resin, 1.5 mol of acrylic acid, 0.0003 mol of hydroquinone and 0.0002 mol of triethylamine into a three-neck flask equipped with a stirrer and a thermometer, raise the temperature to 90°C, and react for 2 hours. Cool down to 50°C, then add 1.5mol aminopropyltriethoxysiloxane, react for 1.5h; add 1.5mol maleic anhydride, 0.0004mol hydroquinone and 0.0002mol triethylamine, Raise the temperature to 95°C at a speed of 1 / min, and react for 2 hours; cool down to 45°C, add 1.5 mol of triethylamine, and continue stirring for 1 hour; the product is obtained.
[0079] The preparation method of waterborne polyurethane acrylate resin is as follows:
[0080] Remove water from 1 moL polybutylene adipate diol (molecular weight: 1000-3000) at 110°C for 1 hour under reduced pressure, then cool down to 80°C, and add 100mL butanone and 0.5moL dimethylol under nitrogen protection Propionic...
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