Preparation method for agricultural nutrient superabsorbent resin
A technology of superabsorbent resin and nutritional type, applied in chemical instruments and methods, applications, agriculture, etc., can solve the problems of lack of nutritional function, high cost of superabsorbent resin, and reduce raw material costs, etc., to achieve good biological and chemical stability, Expand effective utilization and increase water absorption effect
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Embodiment 1
[0026] 1) Weigh 10 parts by weight of dry natural sheep manure, and crush it into 100-mesh powder;
[0027] 2) Disperse 10 parts by weight of kaolin in 20 ml of dimethyl sulfoxide solution, stir and react at 80°C for 24 hours, wash with absolute ethanol three times, and dry in vacuum at 50°C for 8 hours; then disperse it in distilled water and dry Stir to make it swell for 10 minutes, pour it into a three-necked round bottom flask as the first component; then fully dissolve the carboxymethyl starch with distilled water, and transfer it to a separatory funnel to form the second component; at 60°C, Add the second component dropwise to the first component, and react at 80°C for 8 hours after the dropwise addition is completed; after the reaction is completed, filter with suction, wash, and put the sample in a vacuum drying oven to dry at 60°C for 3 hours. Dry at 80°C for 0.5 hours to obtain light gray granules, grind them into fine granules with a mortar, and obtain carboxymethy...
Embodiment 2
[0033] 1) Weigh 15 parts by weight of dry natural sheep manure, and crush it into 100-mesh powder;
[0034]2) Disperse 15 parts by weight of kaolin in 20 ml of dimethyl sulfoxide solution, stir and react at 80°C for 24 hours, wash with absolute ethanol three times, and dry in vacuum at 50°C for 8 hours; then disperse it in distilled water and dry Stir to make it swell for 10 minutes, pour it into a three-necked round bottom flask as the first component; then fully dissolve the carboxymethyl starch with distilled water, and transfer it to a separatory funnel to form the second component; at 60°C, Add the second component dropwise to the first component, and react at 80°C for 8 hours after the dropwise addition is completed; after the reaction is completed, filter with suction, wash, and put the sample in a vacuum drying oven to dry at 60°C for 3 hours. Dry at 80°C for 0.5 hours to obtain light gray granules, grind them into fine granules with a mortar, and obtain carboxymethyl ...
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