Two-effect scale-preventing evaporating and crystallizing device used for evaporating sodium chloride solution and operation method

A sodium chloride solution, evaporative crystallization technology, applied in the direction of alkali metal chlorides, reagents, educts, etc., can solve the problems of difficult operation control, particle material liquid corrosion, and wide application range, so as to achieve smooth feeding and prevent Fouling phenomenon, the effect of realizing continuous and automatic

Active Publication Date: 2012-09-19
南通曙光新能源装备有限公司
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Problems solved by technology

The patent "Ebullating Evaporator with Enhanced Heat Transfer and Anti-fouling Performance and Operation Method" (ZL96120008.1) provides a forced circulation ebullient evaporation device with two separation chambers for two-effect and three-effect operation The structure is complex and the operation is difficult to control
Both of the above two patents mentioned that in the anti-scaling process, the method of adding inert solid particles can be used t...

Method used

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  • Two-effect scale-preventing evaporating and crystallizing device used for evaporating sodium chloride solution and operation method
  • Two-effect scale-preventing evaporating and crystallizing device used for evaporating sodium chloride solution and operation method
  • Two-effect scale-preventing evaporating and crystallizing device used for evaporating sodium chloride solution and operation method

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Embodiment Construction

[0021] The two-effect evaporation crystallization device and operation method of the present invention will be described in detail below in conjunction with the accompanying drawings.

[0022] The solid particles that need to be added are injected into the first effect evaporator and the second effect evaporation crystallizer respectively according to the calculated addition amount, the sodium chloride solution to be evaporated enters the first effect evaporator, open the feeding valve between the effects, and close the outlet Material valve 7, open the vacuum system, so that the vacuum degree of the second effect evaporation crystallizer is maintained at 0.065 ~ 0.09MPa. Introduce raw steam into the first effect heating chamber 1, and maintain the pressure at 0.2-0.35MPa.

[0023] In the case of steam heating, firstly, the sodium chloride solution in the first effect heating chamber 1 forms a natural circulation by relying on the density difference generated after heating, an...

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Abstract

The invention provides a two-effect scale-preventing evaporating and crystallizing device used for evaporating and crystallizing sodium chloride solution, comprising a two-effect multiphase flow evaporator, a vacuum system and a connecting pipeline, wherein a first effect is a natural circular evaporator, a second effect is a natural circular evaporating crystallizer; a material delivering device is arranged between two effects; and the second effect is provided with a grain circulating device. Specially-made aluminum oxide and polytetrafluoroethylene composite material grains are added in the two-effect evaporating and crystallizing device; the grain density is 1200-3000kg/m3, the grain diameter is 0.32-3.8 mm, and the specific heat is 0.5-1.5kJ/kg.K. The sodium chloride crystal is prevented from attaching on the wall face of the heating pipe in the process of evaporating, simultaneously, the heat transmission is enhanced. The two-effect scale-preventing evaporating and crystallizing device has the characteristics of being simple in structure, likely to operate, capable of running continuously and preventing scaling; the two-effect scale-preventing evaporating and crystallizing device can be used for evaporating and crystallizing the sodium chloride solution and the sodium chloride waste liquid in chemical industry, medicine, sea water chemical industry and the other fields.

Description

technical field [0001] The invention relates to an evaporation crystallization technology, in particular to a two-effect anti-scaling evaporation crystallization device for evaporating sodium chloride solution and an operation method thereof, belonging to the field of evaporation crystallization. Background technique [0002] During the evaporation and crystallization process of sodium chloride solution, the crystals produced after the sodium chloride solution is concentrated are easy to adhere to the inner wall of the heating tube to form scaling, which seriously affects the heat transfer and evaporation effects. In order to prevent the scaling of sodium chloride in the heat exchange tubes, multi-effect forced circulation evaporators, reverse circulation evaporators, etc. are widely used at present, but scaling is still inevitable, and frequent cleaning is required, and the cleaning cycle even reaches once or several times a week . [0003] The patent "on-line high-efficie...

Claims

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Application Information

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IPC IPC(8): C01D3/04
CPCY02P20/141
Inventor 邱亚娟赵会兰郭成铁王丽媛
Owner 南通曙光新能源装备有限公司
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