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Process method for producing quartz tube by using solid state method

A process method, quartz tube technology, applied in manufacturing tools, glass forming, glass manufacturing equipment, etc., can solve the problems of complex process, low efficiency, high production cost, achieve obvious doping effect, improve quality and grade, reduce The effect of cumbersome craftsmanship

Inactive Publication Date: 2012-10-10
单祥发
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Problems solved by technology

[0002] At present, the red quartz tube produced by doping rare earth element oxides with high-purity quartz raw material liquid method, the doped rare earth elements and the ratio are copper nitrate (0.1-5%), europium oxide (0.1-5%), magnesium oxide (0.1-5%), etc., after being diluted with a certain amount of water and acid, and then soaked with quartz raw materials, after uniform mixing of liquid rare earth elements and quartz raw materials, high-temperature drying, and gradual cooling, the quartz raw materials and Rare earth elements are uniformly doped, and then put into continuous furnace to produce red quartz tube; the disadvantage is that this liquid doping method has complicated process, high production cost and low efficiency

Method used

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Embodiment Construction

[0021] A process method for producing a quartz tube by a solid state method, comprising:

[0022] (1).Select rare earth element samarium oxide, other related ingredients aluminum nitrate, potassium nitrate, zinc nitrate, barium nitrate, sodium nitrate;

[0023] (2). According to the quantity of quartz molten material in the continuous melting furnace, 0.1 to 15% of samarium oxide, 0.1 to 15% of aluminum nitrate, 0.1 to 15% of potassium nitrate, 0.1 to 15% of zinc nitrate, 0.1 ~15% barium nitrate, 0.1~15% sodium nitrate solid rare earth nitrating agent are evenly mixed;

[0024] (3). A variety of solid rare earth nitrating agents that are uniformly mixed are mixed and stirred for 60 minutes with a turbo mixer;

[0025] (4). A variety of solid rare earth nitrating agents that are evenly stirred are directly added to the continuous melting furnace at high temperature, and a certain amount of quartz raw material has been added to the continuous melting furnace;

[0026] (5). A v...

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Abstract

The invention discloses a process method for producing quartz tubes by using a solid state method. The process method comprises the following steps of: (1) selecting a rare-earth element; (2) uniformly mixing a plurality of kinds of solid rare earth nitration according to the quantity of quartz melting materials inside a continuous melting furnace; (3) mixing and stirring the uniformly mixed rare earth nitration by using a turbine stirring machine; (4) adding the rare earth nitration into the continuous melting furnace directly; (5) adding the rare earth nitration into the continuous melting furnace; (6) continuously rising the temperature of the rare earth nitration and the quartz material; (7) rising the temperature of the continuous melting furnace gradually; (8) keeping the temperature inside the furnace to be black red; (9) generating the black red quartz tube and wholly coloring and shaping; and (10) continuously producing the wholly colored black red quartz tube. The process method has the advantages of simple process and low cost.

Description

technical field [0001] The invention relates to the technical field of inorganic nonmetals, in particular to a process method for producing quartz tubes by a solid state method. Background technique [0002] At present, the red quartz tube produced by doping rare earth element oxides with high-purity quartz raw material liquid method, the doped rare earth elements and the ratio are copper nitrate (0.1-5%), europium oxide (0.1-5%), magnesium oxide (0.1-5%), etc., after being diluted with a certain amount of water and acid, and then soaked with quartz raw materials, after uniform mixing of liquid rare earth elements and quartz raw materials, high-temperature drying, and gradual cooling, the quartz raw materials and Rare earth elements are evenly doped, and then put into a continuous melting furnace to produce red quartz tubes; the disadvantage is that this liquid doping method has complex processes, high production costs, and low efficiency. Contents of the invention [000...

Claims

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Application Information

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IPC IPC(8): C03B20/00
Inventor 单军成
Owner 单祥发
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