Method for detecting sulfur dioxide residue limit of traditional Chinese medicinal material or traditional Chinese medicinal decoction tablet
A technology of decoction pieces of traditional Chinese medicine and sulfur dioxide, which is applied in the direction of analysis using chemical indicators, can solve the problems of complex operation, expensive equipment, and complicated equipment, and achieve the effects of cheap and easy-to-obtain equipment, short reaction time, and easy operation
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Embodiment 1
[0052] Embodiment 1 The equipment used in the detection method of the present invention
[0053] Such as figure 1 As shown, the equipment includes a conical flask 1, an airway 2, a cock 3, and a cock cover 4, wherein the airway 2 is connected to the conical flask 1 through a grinding port; the center of the cock 3 has a round hole, and the airway 2 Put it into the round hole of the cock 3; there is a round hole in the center of the cock cover 4, which is placed on the cock 3 and coincides with the cock 3; The outer diameter is compatible; the top of the cock 3 is a circular plane.
[0054] A 100ml standard ground-mouth Erlenmeyer flask 1 can be taken, connected to the upper airway 2 (outer diameter 8.0mm, inner diameter 6.0mm, total length 180mm), which can also be connected with a ground-mouth adapter; the upper part of the plexiglass cock 3 is a round There is a circular hole in the center, the diameter of which is consistent with the inner diameter of the airway tube 2, a...
Embodiment 2
[0055] Embodiment 2 detection method of the present invention
[0056] Adopt the equipment described in embodiment 1, put a piece of lead acetate test paper on the top plane of cock 3, the test paper size is advisable to cover the aperture and not expose outside the plane, cover the cock cover 4, and tighten; take the Chinese medicinal material to be tested Or Chinese medicine decoction pieces are placed in the conical flask 1, after adding water, zinc particles, hydrochloric acid solution, immediately install the airway 2, the cock 3 with the lead acetate test paper, the cock cover 4, react for 40 minutes, take out the lead acetate test paper, and mix with Standard color comparison card is used to determine the limit of residual sulfur dioxide. The operation steps are as follows:
[0057] (1) Preparation of standard color chart
[0058] The pipetting concentration was 0.4mg·ml -1 , 0.3mg·ml -1 , 0.15mg·ml -1 、0mg·ml -1 Put 0.1ml of sulfur dioxide standard solution in the...
Embodiment 3
[0078] The condition investigation of embodiment 3 detection method of the present invention
[0079] 1. Instruments and materials
[0080] 1.1 Instrument
[0081] BP211D electronic balance (one hundred thousandth, German Sartorius company)
[0082] UPT-I-10T type Youpu UPT series ultrapure water device (Chengdu Ultrapure Technology Co., Ltd.)
[0083] DSY-1-2 hole constant temperature water bath (Beijing Guohua Medical Instrument Factory)
[0084] IXUS80 digital camera (Canon, 8 million pixels)
[0085] Rapid Determination Device for Residual Sulfur Dioxide (Patent No.: G01N21 / 78)
[0086] 1.2 Reagents and Reagents
[0087] Sodium bisulfite (Sinopharm Chemical Reagent Co., Ltd., content ≥99.8%);
[0088] Hydrochloric acid (AR, 36-38% HCL, Chengdu Kelong Chemical Reagent Factory);
[0089] Zinc particles (Sinopharm Chemical Reagent Co., Ltd., content ≥99.5%);
[0090] Lead acetate (Sinopharm Chemical Reagent Co., Ltd., content ≥99.8%);
[0091] Acetic acid (AR, Chengd...
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Abstract
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