Gas phase polyethylene device quality index and operational constraint on-line estimation system and method thereof

A quality index, polyethylene technology, applied in the direction of electrical program control, comprehensive factory control, comprehensive factory control, etc., can solve the problems of difficult long-term operation, difficult to adapt to brand switching, etc.

Active Publication Date: 2014-07-16
BEIJING UNIV OF CHEM TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] In order to overcome the limitations of the existing quality index and operating constraint estimation technology used in the gas phase PE process, which is difficult to adapt to frequent brand switching and widespread unknown interference, and thus difficult to run for a long period of time, the present invention provides a method for gas phase fluidized bed production. The online estimation system and method of polyethylene (PE) multi-brand product quality indicators and operational constraints, the key point of which is: combining the strengths of the mixed model modular design method and the semi-parametric design method, the quality of the gas phase PE process is constructed. The prediction model of the index and operation constraints; the self-adaptive adjustment of the quality index prediction model when the brand is switched is realized by using the module reverse push adaptive method; the robust suboptimal filtering considering the approximation deviation and process uncertainty of the quality index prediction model is used Estimation method, combined with laboratory analysis data, realizes real-time estimation of PE multi-brand product quality indicators and operational constraints

Method used

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  • Gas phase polyethylene device quality index and operational constraint on-line estimation system and method thereof
  • Gas phase polyethylene device quality index and operational constraint on-line estimation system and method thereof
  • Gas phase polyethylene device quality index and operational constraint on-line estimation system and method thereof

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Embodiment 1

[0103] Apply the present invention to a linear low density polyethylene (LLDPE) production unit, the device process flow is with reference to image 3 . The device adopts the low-pressure gas-phase polyethylene process technology of United Carbon Corporation. The device is composed of raw material refining, polymerization reaction, resin degassing, tail gas recovery, additive treatment, granulation, air delivery and packaging. The original design capacity was 100,000 tons / year of polyethylene resin. After the third-phase transformation, the current production capacity of the device has been expanded to 274,000 tons / year. refer to figure 1 , figure 2 , an on-line estimation system for gas-phase polyethylene plant quality indicators and operational constraints, including field instruments connected to the LLDPE plant, Honeywell TDC3000DCS system (where the APP Node is used as the OPC Server), the database of the laboratory analysis data server is the PI database and the ethyl...

Embodiment 2

[0112] The present invention is applied to the gas-phase method polyethylene multi-brand industrial pilot test evaluation device, and the process flow of the production device is referred to Figure 16 . The multi-brand industrial pilot test evaluation device is used to evaluate the performance of the gas phase PE catalyst and the parameters of the multi-brand PE industrial production process. The device adopts the production process of continuous gas phase polymerization, and the design capacity is 5kg / hr. The main body of the device includes raw material and catalyst feeding system, gas phase reactor system, polymer separation system, back blowing gas system, etc.; it is equipped with raw material purification system, instrument air system, cooling water system, discharge system, etc., of which the instrument air system and cooling water system It is shared with the loop pipe pilot plant in the workshop, and the high-purity nitrogen, steam, circulating water, etc. used by t...

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Abstract

The invention provides a polyethylene (PE) multi-trademark product quality index and operational constraint on-line estimation system for gas phase fluidized bed production technology. The system comprises a field process instrument which is connected with a gas phase PE object, a field analysis instrument, a distributed control system (DCS), a laboratory analysis data server and an advanced control server. The advanced control server includes an OPC client, a data interface module, a multi-trademark PE production process quality indicator and operational constraint model prediction module, a PE quality index prediction model parameter adaptive correction module, and a PE quality index robustness suboptimal filter estimation and quality indicator and operational constraint display module. The invention also provides a gas phase PE quality index and operational constraint on-line estimation method. The invention provides the real-time online estimation system and method of multi-trademark gas phase PE product quality index melt index and density, gas phase PE production operating constraint yield, and recycle gas dew point temperature.

Description

technical field [0001] The invention relates to the field of industrial process control, and is an online estimation system for the quality index and operation constraints of a polyethylene device for a gas-phase fluidized bed production process. Background technique [0002] Polyethylene (PE) is the most productive variety among polyolefins. As a thermoplastic polymer, it is widely used in various fields of the national economy such as industry, agriculture, national defense, and daily necessities. At present, polyethylene accounts for 70% of the world's total consumption of polyolefins, 44% of the total consumption of thermoplastic general-purpose resins, and the raw materials used account for 52% of the world's ethylene consumption. 70% of the output (Qian Bozhang. The technical progress of contemporary polyethylene production. International Chemical Information, 2002, 1: 9-11.). The polyethylene production process of the gas phase process includes five reversible reacti...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G05B19/418
CPCY02P80/40Y02P90/02
Inventor 赵众孙康
Owner BEIJING UNIV OF CHEM TECH
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