Composite porous electrode, single cell comprising composite porous electrode, cell stack and preparation method of composite porous electrode
A porous electrode and flow battery technology, which is applied in battery electrodes, regenerative fuel cells, fuel cell grouping, etc. Effect of resistance and low contact resistance
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[0032] In a specific embodiment of the present invention, when the resin material is a thermoplastic resin composition, the preparation method includes the following steps: A1. Dissolving the resin material in a solvent to form a resin with a mass concentration of the resin material of 0.5-20% material solution; A2, immersing the porous electrode 3' in the resin material solution, so that the resin material solution is immersed in the pores of the porous electrode body 3'; and A3, volatilizing the solvent in the porous electrode body 3', so that the resin material adheres A resin layer is formed on the inner walls of the pores of the porous electrode body 3 ′ to obtain the composite porous electrode 3 .
[0033] The resin material is dissolved in its good solvent to form a resin material solution, and then the porous electrode body 3' is immersed in the resin material solution. The solvent used is volatilized, and after the solvent is volatilized, the resin material can form a...
Embodiment 1
[0044] Raw material: graphite felt is used as the porous electrode body, the porosity is 85%, and the external dimension is 36mm*36mm*8mm. Polystyrene is selected as the impregnating resin, and the solvent is dimethylformamide.
[0045] Preparation process: first dissolve the polystyrene resin in dimethylformamide to form a solution with a mass concentration of 1%; then immerse the graphite felt into the solution, and after the solution is evenly dipped into the graphite felt, slowly heat to 155 ℃, keep it for 6h to make the dimethylformamide gradually and completely volatilize; then slowly cool to 25℃ to precipitate and solidify the polystyrene, that is, a composite porous electrode with a polystyrene resin impregnated with graphite felt is obtained, and the total weight of the resin layer is obtained. 0.8% of the total weight of the composite porous electrode.
[0046] The single cell of Example 1 was obtained by assembling the current collector plate, the flow frame, the s...
Embodiment 2
[0048] Raw material: graphite felt is used as the porous electrode body, the porosity is 85%, and the external dimension is 36mm*36mm*8mm. High-density polyethylene is used as the impregnating resin, and the solvent is xylene.
[0049] Preparation process: first dissolve polyethylene resin in xylene to form a solution with a mass concentration of 8wt%; then immerse the graphite felt into the solution, and after the solution is evenly immersed into the graphite felt, slowly heat to 50°C for 6h The solvent is gradually and completely volatilized; and then slowly cooled to 25° C. to precipitate and solidify the polyethylene resin, that is, a composite porous electrode with an integrally impregnated graphite felt with a high-density polyethylene resin is obtained, and the total weight of the resin layer is 5% of the total weight of the obtained composite porous electrode. %.
[0050] The single cell of Example 2 was obtained by assembling the current collector plate, the flow fra...
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