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High-oxygen resistant steaming-resistant polyvinylidene chloride coating film and manufacturing method thereof

A technology of polyvinylidene chloride and vinylidene chloride, which is applied to chemical instruments and methods, devices for coating liquid on surfaces, coatings, etc., and can solve problems such as easy pinholes

Active Publication Date: 2015-04-29
HAINAN SHINER IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] In response to the above problems, the object of the present invention is to provide a high oxygen resistance and retort resistant polyvinylidene chloride coating film, which is modified with the high oxygen resistance and retort resistance polyvinylidene chloride latex of the present invention It is an organic coating, which effectively solves the disadvantage of easy pinholes when using aluminum foil as a composite layer. It can withstand high-temperature cooking and does not turn white or yellow. It is also safe and environmentally friendly, and has excellent oxygen barrier properties.

Method used

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  • High-oxygen resistant steaming-resistant polyvinylidene chloride coating film and manufacturing method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] Substrate: biaxially oriented polyester (BOPET), thickness 12 μm.

[0033] Nano material filler 7.5kg

[0034] Main agent: commercially available main agent 17.5kg

[0035] Curing agent: commercially available curing agent 3.5kg

[0036] Solvent: commercially available solvent 70kg

[0037] Polyvinylidene chloride emulsion: self-made polyvinylidene chloride emulsion 175kg

[0038] Softened water: 300kg

[0039] Slip agent: commercially available palm wax slip agent 3kg

[0040] Anti-blocking agent: 2.5kg of commercially available silicon dioxide anti-blocking agent

[0041] Weigh 175kg of the above-mentioned polyvinylidene chloride blended emulsion and add it to a stainless steel container, while stirring, add 3kg of palm wax slip agent, 7.5kg of nanomaterial filler, 2.5kg of silicon dioxide anti-sticking agent and 300kg of softening agent. water, stir evenly to form a modified retort-resistant polyvinylidene chloride emulsion, which is used in the coating process...

Embodiment 2

[0047] Substrate: biaxially oriented polyester (BOPET), thickness 12 μm.

[0048] Nano material filler 24kg

[0049] Main agent: commercially available main agent 20kg

[0050] Curing agent: commercially available curing agent 4kg

[0051] Solvent: commercially available solvent 80kg

[0052] Polyvinylidene chloride emulsion: self-made polyvinylidene chloride emulsion 200kg

[0053] Softened water: 152kg

[0054] Slip agent: commercially available palm wax slip agent 4kg

[0055] Anti-blocking agent: commercially available silica anti-blocking agent 20kg

[0056] Take by weighing 200kg above-mentioned polyvinylidene chloride blended emulsion that makes and add in the stainless steel container, add 4kg palm wax slippery agent, 24kg nanometer material filler, 20kg silicon dioxide antisticking agent and 152kg demineralized water successively while stirring, After stirring evenly, the modified retort-resistant polyvinylidene chloride emulsion is ready to be used in the coati...

Embodiment 3

[0062] Substrate: biaxially oriented polyester (BOPET), thickness 12 μm.

[0063] Nano material filler 5kg

[0064] Main agent: commercially available main agent 8.8kg

[0065] Curing agent: commercially available curing agent 1.76kg

[0066] Solvent: commercially available solvent 35.2kg

[0067] Polyvinylidene chloride emulsion: self-made polyvinylidene chloride emulsion 88kg

[0068] Demineralized water: 5.9kg

[0069] Slip agent: commercially available palm wax slip agent 1kg

[0070] Anti-blocking agent: 0.1kg of commercially available silicon dioxide anti-blocking agent

[0071] Weigh 88kg of the above-mentioned polyvinylidene chloride blended emulsion and add it to a stainless steel container, while stirring, add 1kg of palm wax slip agent, 5kg of nanomaterial filler, 0.1kg of silicon dioxide anti-sticking agent and 5.9kg of softening agent successively. water, stir evenly to form a modified retort-resistant polyvinylidene chloride emulsion, which is used in the c...

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Abstract

The invention relates to a high-oxygen resistant steaming-resistant polyvinylidene chloride coating film and a manufacturing method thereof. The high-oxygen resistant steaming-resistant polyvinylidene chloride coating film comprises a base, a coating layer on the surface of the base, and a base glue layer between the coating layer and the base. The coating layer is a coating obtained by coating modified high-oxygen resistant steaming-resistant polyvinylidene chloride latex. The modified high-oxygen resistant steaming-resistant polyvinylidene chloride latex comprises: by weight, 30 to 38% of a high-oxygen resistant steaming-resistant polyvinylidene chloride blended emulsion, 1.5 to 6% of a nano-material filler, 1 to 8% of a slip agent, 0.1 to 5% of an abherent and 5 to 60% of softened water. The high-oxygen resistant steaming-resistant polyvinylidene chloride blended emulsion comprises: by weight, 40 to 94% of a vinylidene chloride monomer, 1.5 to 10% of an acrylate, 1 to 6% of one or more of acrylic acid and acrylonitrile, 0.5 to 2% of an initiator, 0.1 to 0.8% of an emulsifier, 0.5 to 1% of a stabilizer and 0 to 55% of soft water.

Description

Technical field [0001] The invention relates to a polyvinylidene chloride coating film with high oxygen resistance and cooking resistance and a manufacturing method thereof, belonging to the field of new polymer materials. Background technique [0002] Glass bottles and metal filling have been the main way of food storage for a long time in the past. In 1958, the soft can packaging developed by the United States successfully replaced tinplate cans, and commercialized large-scale production began. Since 1968, Japan began to use high-temperature cooking For bag-packed curry food, rice, meatballs, etc., high-temperature cooking and sterilization has become a common method to extend the shelf life of food. Problems such as bag swelling, bag breaking, odor, delamination, surface wrinkling, curling, air leakage, and pinholes have caused quality disputes. At present, in the selection of high-temperature retort bag materials, in addition to solving the above problems, safety and en...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B32B27/08B32B27/30B32B7/12C09D127/08C09D7/12C08F214/08C08F220/14C08F220/06C08F220/44C08F2/26B05D1/38B05D3/02
Inventor 王恩飞洪景利
Owner HAINAN SHINER IND
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