Curable resin composition, adhesive epoxy resin paste, die-bonding agent, non-conductive paste, adhesive epoxy resin film, non-conductive epoxy resin film, anisotropic conductive paste, and anisotropic conductive film
A technology of curable resin and epoxy resin, applied in the direction of conductive materials dispersed in non-conductive inorganic materials, epoxy resin glue, adhesive type, etc., can solve the cracking of conduction resistance adhesive and poor thermal expansion rate , high elastic modulus, etc., to achieve high conduction reliability and maintain the effect of crack resistance
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[0042] 1-6. Preparation method of curable resin composition
[0043] 2. Other embodiment using curable resin composition
[0044] 3. Examples.
[0045]
[0046] The curable resin composition of the present embodiment contains an epoxy resin and a curing agent for an epoxy resin, and the difference between the maximum value of tan δ in the viscoelastic spectrum and the value of tan δ at −40° C. is 0.1 or more.
[0047] The tan δ (loss tangent value) refers to a value of 0 or more and less than 1 calculated by the formula represented by tan δ=E'' / E'. Among them, E'' is the loss elastic modulus, and E' is the storage elastic modulus. Tanδ is calculated as follows, for example, by measuring the viscoelastic spectrum of the storage elastic modulus (E') and the viscoelastic spectrum of the loss elastic modulus (E'') within a predetermined temperature range with a viscoelasticity testing machine, From this, tan δ was calculated from the above formula. The larger the value of ta...
Embodiment
[0094] Specific examples of the present invention will be described below. Moreover, any one of the following examples does not limit the scope of the present invention.
[0095]
[0096] ·Acrylic
[0097] Ethyl Acrylate (EA100), Glycidyl Methacrylate (GMA10)
[0098] ·Epoxy resin
[0099] 1,3,5-Triglycidyl isocyanurate (manufactured by TEPIC Nissan Chemical Industry Co., Ltd.), alicyclic epoxy resin (manufactured by CEL Hitachi Chemical Co., Ltd.), glycidyl hexahydrobisphenol A (manufactured by YX8000 JER Co., Ltd. ), dicyclopentadiene type liquid epoxy resin (EP4088SS)
[0100] ·Hardener
[0101] Methylhexahydroxyphthalic anhydride (MeHHPA, Nippon Chemical Co., Ltd.), diethylglutaric anhydride (Degan, Kyowa Hakka Chemical Co., Ltd.)
[0102] ·Curing Accelerator
[0103] 2-Ethyl-4-methylimidazole (2E4MZ manufactured by Shikoku Chemical Industry Co., Ltd.)
[0104] ·Conductive particles
[0105] Particles made by plating Ni / Au on 5 μm cross-linked polystyrene resin p...
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Abstract
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